4,4'-二苯基-2-丁酮合成路线 (共 85 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium(II) oxide hydrate; trifluoroacetic acid in 1,4-dioxane; water T=120°C; P=760.051 Torr; 20 h; Inert atmosphere;
参考文献
Chen, Wen; Zhou, Xianya; Xiao, Fuhong; Luo, Jiaying; Deng, Guo-Jun
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4347 - 4350
反应条件
dimethylphenylsilane; C19H8O7Ru3 in 1,4-dioxane T=50°C; 3 h; Inert atmosphere;
参考文献
Harada, Nari-Aki; Nishikata, Takashi; Nagashima, Hideo
Tetrahedron, 2012 , vol. 68, # 15 p. 3243 - 3252
反应条件
potassium phosphate; phosphite-based type I palladacycle in toluene T=20°C;
参考文献
He, Ping; Lu, Yong; Hu, Qiao-Sheng
Tetrahedron Letters, 2007 , vol. 48, # 30 p. 5283 - 5288
反应条件
tributyl-amine; tetra-(n-butyl)ammonium iodide; trifluoroacetic acid; [Pd(PPh3)2(OAc)2] in N,N-dimethyl-formamide T=70°C;
参考文献
Amorese, A.; Arcadi, A.; Bernocchi, E.; Cacchi, S.; Cerrini, S.; et al.
Tetrahedron, 1989 , vol. 45, # 3 p. 813 - 828
反应条件
potassium phosphate; platinacycle in toluene T=90 - 95°C;
参考文献
Tang, Yi-Qiang; Lv, Huan; He, Xiao-Na; Lu, Jian-Mei; Shao, Li-Xiong
Catalysis Letters, 2011 , vol. 141, # 5 p. 705 - 708
反应条件
water; [Rh(NCMe)2(cod)][BF4] in tetrahydrofuran T=60°C; 2 h;
参考文献
Oi, Shuichi; Moro, Mitsutoshi; Ito, Hisanori; Honma, Yoshio; Miyano, Sotaro; Inoue, Yoshio
Tetrahedron, 2002 , vol. 58, # 1 p. 91 - 97
反应条件
Cu(BF4)2; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane; water T=75°C; 23 h;
参考文献
Nishikata, Takashi; Yamamoto, Yasunori; Miyaura, Norio
Chemistry Letters, 2003 , vol. 32, # 8 p. 752 - 753
反应条件
formic acid; triethylamine; [Pd(PPh3)2(OAc)2] in acetonitrile T=80°C; 12 h;
参考文献
Synthesis, , # 7 p. 575 - 577
反应条件
1: Poly(phenylmethylsiloxane) With potassium carbonate in toluene T=20°C; 1 h; 2: (E)-4-phenyl-3-buten-2-one With water; [Rh(OH)(cycloocta-1,5-diene)]2 in toluene T=120°C; 24 h;
参考文献
Koike, Tooru; Du, Xiaoli; Mori, Atsunori; Osakada, Kohtaro
Synlett, 2002 , # 2 p. 301 - 303
反应条件
bis(acetylacetonato) palladium; oxygen in 1,4-dioxane; water T=80°C; P=760.051 Torr; 24 h; Reagent/catalystSolvent;
参考文献
Chen, Wen; Chen, Hui; Xiao, Fuhong; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 26 p. 4295 - 4298