2-(4-叔丁基苯)乙醇合成路线 (共 18 条)
反应条件
1: p-TsOH*H2O 2: 87 percent / LiAlH4 / diethyl ether / 0.5 h / Heating View Scheme
参考文献
Farmaco, , vol. 54, # 10 p. 684 - 694
反应条件
1: H2O / methanol 2: p-TsOH*H2O 3: 87 percent / LiAlH4 / diethyl ether / 0.5 h / Heating View Scheme
参考文献
Farmaco, , vol. 54, # 10 p. 684 - 694
反应条件
n-butyllithium; potassium tert-butylate 1.) THF, hexane, -50 deg C, 3 h, 2.) THF, hexane, 25 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 415, # 1 p. 1 - 6
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 43, p. 241
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 60, p. 352
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 9, p. 99,103
反应条件
Dess-Martin periodane in chloroform T=20°C; 3 h; Cooling with ice;
参考文献
EP2687507 A1, ;
Paragraph 0264 ;
反应条件
Potassium peroxomonosulfate; MnCl2∙4H2O; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in acetone T=0 - 20°C; 4 h; chemoselective reaction;
参考文献
Synthesis, , # 14 art. no. E27210SS, p. 2475 - 2489
反应条件
Potassium peroxomonosulfate; MnCl2∙4H2O; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in acetone T=0 - 20°C; 4 h; chemoselective reaction;
参考文献
Synthesis, , # 14 art. no. E27210SS, p. 2475 - 2489