3-(4-甲氧苯基)-1-丙醇合成路线 (共 74 条)
反应条件
1: K2CO3, 18-crown-6 / acetone / Heating 2: 24 percent / Bu3SnH, AIBN / benzene / 1 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 14 p. 2343 - 2346
反应条件
1: 76 percent 2: 80 percent / NaBH4 / tetrahydrofuran / 1) 0 deg C, 2 h, 2) rt, 2 h View Scheme
参考文献
Tetrahedron, , vol. 48, # 21 p. 4431 - 4438
参考文献
Proceedings of the Koninklijke Nederlandse Akademie van Wetenschappen, Series B: Physical Sciences, , vol. 40, p. 706
Recueil des Travaux Chimiques des Pays-Bas, , vol. 57, p. 233
反应条件
3-(4-methoxyphenyl)propionaldehyde; magnesium in tetrahydrofuran
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
反应条件
1: 59 percent / lithium aluminium hydride / diethyl ether 2: 62 percent / pyridine 3: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature 4: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
反应条件
1: 62 percent / pyridine 2: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature 3: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
反应条件
1: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature 2: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
反应条件
1: pyridinium chlorochromate / dichloromethane 2: sodium hydride / tetrahydrofuran 3: hydrogen; palladium on activated charcoal / ethyl acetate 4: lithium aluminium tetrahydride / tetrahydrofuran View Scheme
参考文献
Chemistry Letters, , vol. 42, # 9 p. 1051 - 1052
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 51, p. 108,117
反应条件
magnesium in tetrahydrofuran
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622