2-羟基-4-氧代-2-戊酸合成路线 (共 3 条)
反应条件
1: With titanium(IV) isopropylate; 4 A molecular sieve; (+)-Weinsaeure-diethylester in dichloromethane
T=-20°C; 0.5 h;
2: With tert.-butylhydroperoxide in decane; dichloromethane
T=-20°C; 42 h;
3: With titanium(IV) isopropylate; tert.-butylhydroperoxide
参考文献
Paju, Anne; Kanger, Tonis; Pehk, Tonis; Lindmaa, Rasmus; Mueuerisepp, Aleksander-Mati; Lopp, Margus
Tetrahedron Asymmetry, 2003 , vol. 14, # 11 p. 1565 - 1573
反应条件
sodium tetrahydroborate
参考文献
Guthrie,J.P.
Journal of the American Chemical Society, 1972 , vol. 94, p. 7024 - 7029
反应条件
sulfuric acid
4 h; Heating;
参考文献
Lueoend, Rainer M.; Walker, Josef; Neier, Reinhard W.
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 5005 - 5013