N,N-二甲基苄基胺 N-氧化物合成路线 (共 15 条)
反应条件
DAL T=0°C; Yield given. Yields of byproduct given;
参考文献
Beugelmans, Rene; Benadjila-Iguertsira, Leila; Chastanet, Jacqueline; Negron, Guillermo; Roussi, Georges
Canadian Journal of Chemistry, 1985 , vol. 63, p. 725 - 734
反应条件
T=127°C; Rate constant;
参考文献
Lorand, John P.; Anderson, James L.; Shafer, Brian P.; Verral, Daniel L.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1560 - 1563
反应条件
1: 1.) MeLi, 2.) TiCl4 / 1.) CH2Cl2, THF; 2.) CH2Cl2, -78 deg C, 1 h 2: Ambient temperature View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 3 p. 735 - 740
反应条件
indium; ammonium chloride in methanol; water Reduction; 3 h; Heating;
参考文献
Tetrahedron Letters, , vol. 41, # 15 p. 2663 - 2665
反应条件
AFA in dichloromethane T=0 - 21°C;
参考文献
Chemistry Letters, , p. 1517 - 1520
反应条件
T=127°C; Rate constant;
参考文献
Journal of Organic Chemistry, , vol. 58, # 6 p. 1560 - 1563
反应条件
4a-hydroperoxy-5-ethyl-3-methyllumiflavin in tert-butyl alcohol
T=30°C; Rate constant;
参考文献
Ball, Sheldon; Bruice, Thomas C.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6498 - 6503
反应条件
oxygen in methanol; water
T=116°C; P=53254.2 Torr; 7 h;
参考文献
Riley, Dennis P.; Correa, Paul E.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1563 - 1564
反应条件
in N,N-dimethyl-formamide
T=30°C; Rate constant;
参考文献
Ball, Sheldon; Bruice, Thomas C.
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5494 - 5503
反应条件
in N,N-dimethyl-formamide
T=30°C; Rate constant;
参考文献
Ball, Sheldon; Bruice, Thomas C.
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5494 - 5503