N-(4-溴丁基)邻苯二甲酰亚胺合成路线 (共 50 条)
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate in acetone T=20°C; 24 h;
参考文献
Hou, Duen-Ren; Cheng, Hsiu-Yi; Wang, Eng-Chi
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 6094 - 6099
参考文献
Gillet, Jean-Philippe; Ruppin, Chirstophe
Patent: US2004/176613 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
carbon tetrabromide; triphenylphosphine in acetonitrile T=20°C; 2.5 h;
参考文献
WO2011/121055 A1, ;
Page/Page column 24 ;
WO 2011/121055 A1
反应条件
sodium hydrogencarbonate in N-methyl-acetamide; hexane; water
参考文献
Chen, Gang; Crawford, Jason; Skerlj, Renato
Patent: US2005/154201 A1, 2005 ;
反应条件
phosphorus tribromide in water; isopropyl alcohol; toluene
反应条件
potassium carbonate T=160 - 165°C; 4 h;
参考文献
Russian Journal of Applied Chemistry, , vol. 73, # 12 p. 2106 - 2108
反应条件
1: potassium hydroxide / ethanol; water / Reflux 2: N,N-dimethyl-formamide / 12 h / 100 °C View Scheme
参考文献
Organic Letters, , vol. 13, # 4 p. 764 - 767
反应条件
1: 140 °C 2: carbon tetrabromide; triphenylphosphine / acetonitrile / 2.5 h / 20 °C View Scheme
参考文献
WO2011/121055 A1, ;
WO 2011/121055 A1
反应条件
potassium carbonate in acetonitrile 24 h; Heating;
参考文献
Xu, Songbo; Podoprygorina, Ganna; Boehmer, Volker; Ding, Zhifeng; Rooney, Patrick; Rangan, Chitra; Mittler, Silvia
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 3 p. 558 - 568
参考文献
Ashley et al.
Journal of the Chemical Society, 1959 , p. 3880,3882