1: n-butyllithium With anhydrous iron chloride in hexanes
T=-78°C; 3 h; Inert atmosphere;
2: benzophenone in hexanes
T=-78 - 25°C; 15 h; Inert atmosphere;
3: With hydrogenchloride; water in hexanes
参考文献
Eisch, John J.; Sohn, Jane U.; Rabinowitz, Edon J.
European Journal of Organic Chemistry, 2010 , # 15 p. 2971 - 2977