4,4'-亚甲基双(2,6-二甲苯酚)合成路线 （共 37 条）
反应条件
hydrogenchloride in light petroleum; water T=27°C;
参考文献
Singh, Deepak; Chaudhari, Umesh V.; Deota, Pradeep T.
Tetrahedron, 2014 , vol. 70, # 30 p. 4485 - 4493
反应条件
ammonium acetate; potassium hexacyanoferrate(III) in methanol; water T=45°C; 240 h;
参考文献
Goldstein, Stephen L.; McNelis, Edward
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1613 - 1620
参考文献
Arkiv foer Kemi, , vol. 15 A, # 7 p. 7
反应条件
sodium hydroxide 18 h; Ambient temperature; Yields of byproduct given;
参考文献
Massy, D. J. R.; McKillop, A.
Synthesis, 1989 , # 4 p. 253 - 255
反应条件
potassium hydroxide in water T=100°C; 2 h; Further byproducts given;
参考文献
Journal of Chemical Research, Miniprint, , # 3 p. 701 - 770
反应条件
1: n-PrNH2 / 24 h / Heating 2: KOH / H2O / 2 h / 100 °C View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 3 p. 701 - 770
反应条件
1: aqueous NaOH 2: 180 °C / 1 Torr View Scheme
参考文献
Chemische Berichte, , vol. 74, p. 1533,1537
反应条件
dichloromethane T=15°C; 48 h; Irradiation;
参考文献
Polish Journal of Chemistry, , vol. 54, # 5 p. 1073 - 1080
反应条件
1: allyl alcohol With sodium hydroxide T=90 - 100°C; 0.5 h; Inert atmosphere; 2: 2-hydroxy-1,3-dimethylbenzene T=135°C; 18 h; Inert atmosphere;
参考文献
Krysin; Khalikova; Khlebnikova; Nogina; Mamatyuk
Russian Journal of General Chemistry, 2010 , vol. 80, # 11 p. 2290 - 2297
反应条件
1: 1.) SnCl4, 2.) Raney Ni / 1.) CH2Cl2, room temp., 1 h, 2.) acetone, ethanol, room temp., 1 h 2: 1.) SnCl4, 2.) Raney Ni / 1.) CH2Cl2, room temp., 1 h, 2.) acetone, ethanol, room temp., 1 h View Scheme
参考文献
Synthesis, , # 11 p. 937 - 939
