4'-甲基-3-硝基联苯合成路线 (共 38 条)
参考文献
Goossen, Lukas J.; Zimmermann, Bettina; Knauber, Thomas
Angewandte Chemie - International Edition, 2008 , vol. 47, # 37 p. 7103 - 7106
反应条件
hydroquinone in toluene
Heating;
参考文献
Podgornova,N.N. et al.
Journal of Organic Chemistry USSR (English Translation), 1974 , vol. 10, p. 1993 - 1994
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, # 9 p. 1985 - 1986
反应条件
1: 1.) 1 M aq. HCl, NaNO2 / 1.) 0 deg C, 30 min, 2.) 0 deg C, 30 min
2: CF3COOH / 3 h / 65 - 70 °C
View Scheme
参考文献
Patrick, Timothy B.; Willaredt, Richard P.; DeGonia, David J.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2232 - 2235
反应条件
sulfuric acid; hypophosphorous acid
Diazotization;
参考文献
Hey et al.
Journal of the Chemical Society, 1951 , p. 2892,2902
反应条件
1: acetic acid; H2SO4; HNO3
2: aqueous H2SO4
3: aqueous H2SO4; aqueous H3PO2 / Diazotization
View Scheme
参考文献
Hey et al.
Journal of the Chemical Society, 1951 , p. 2892,2902
反应条件
1: aqueous H2SO4
2: aqueous H2SO4; aqueous H3PO2 / Diazotization
View Scheme
参考文献
Hey et al.
Journal of the Chemical Society, 1951 , p. 2892,2902
反应条件
tert-Butyl thionitrate
1 h; Heating; Title compound not separated from byproducts;
参考文献
Oae, Shigeru; Shinhama, Koichi; Kim, Yong Hae
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 7 p. 2023 - 2026
参考文献
Makarowa et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 1452,1457; engl. Ausg. S. 1399, 1404