N~1~,N~1~-二甲基-4-硝基-1,2-苯二胺合成路线 (共 10 条)
参考文献
Chemische Berichte, , vol. 21, p. 2306
反应条件
1: 83 percent / copper(II) acetate / dimethylformamide / 100 °C 2: SOCl2, DMF / 1,2-dichloro-ethane / 0.5 h / Heating 3: CH2Cl2 / 0.08 h 4: 34 percent / POCl3 / 4 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 32, # 1 p. 23 - 30
反应条件
sodium sulfide in ethanol; water
0.5 h; Heating;
参考文献
Wilson; Anderson; Denny
Journal of Medicinal Chemistry, 1989 , vol. 32, # 1 p. 23 - 30
反应条件
in ethanol
T=20°C; 480 h;
参考文献
De Castro, Sonia; Chicharro, Roberto; Aran, Vicente J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 6 p. 790 - 802
参考文献
Heim
Chemische Berichte, 1888 , vol. 21, p. 2306
反应条件
1: acetic acid; nitric acid
2: tin (II)-chloride; hydrogen chloride; ethanol
View Scheme
参考文献
Ayling; Gorvin; Hinkel
Journal of the Chemical Society, 1942 , p. 755,756
参考文献
Heim
Chemische Berichte, 1888 , vol. 21, p. 2306
参考文献
Ayling; Gorvin; Hinkel
Journal of the Chemical Society, 1942 , p. 755,756
反应条件
1: 97 percent / acetone / 1 h / 20 °C
2: 98 percent / nitromethane / 24 h / Heating
View Scheme
参考文献
De Castro, Sonia; Chicharro, Roberto; Aran, Vicente J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 6 p. 790 - 802
参考文献
Ayling; Gorvin; Hinkel
Journal of the Chemical Society, 1942 , p. 755,756