2-氨基-1,3-丙二醇合成路线 （共 34 条）
反应条件
ammonium hydroxide; hydrogen in methanol; water T=65°C; P=12929 Torr; 6 h; Autoclave; Reagent/catalyst;
参考文献
Penn A Kem LLC; Hegde, Shridhar G.; Zhao, Lei
Patent: US8653306 B1, 2014 ;
Location in patent: Page/Page column 3-4 ;
反应条件
methanol T=20°C; 12 h;
参考文献
GLOBAL AGRITECH INC
Patent: WO2008/147671 A2, 2008 ;
Location in patent: Page/Page column 55 ;
反应条件
hydrogen; Nishimura catalyst <(45.9percent Rh/19.9percent Pt) oxide> in methanol T=25°C; P=75007.5 Torr;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 8 p. 802 - 808
反应条件
ethanol; nickel T=100°C; P=250073 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 3121
反应条件
sodium cyanoborohydride; ammonium chloride; acetic acid in methanol T=20°C;
参考文献
Jie, Yuanping; Livant, Peter; Li, Hui; Yang, Minmin; Zhu, Wei; Cammarata, Vince; Almond, Philip; Sullens, Tyler; Qin, Yu; Bakker, Eric
Journal of Organic Chemistry, 2010 , vol. 75, # 13 p. 4472 - 4479
反应条件
potassium borohydride in methanol; water T=20°C; 12 h;
参考文献
Gu, Keli; Bi, Lanrong; Zhao, Ming; Wang, Chao; Dolan, Cheryl; Kao, Michael C.; Tok, Jeffrey B.-H.; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 5 p. 1339 - 1347
反应条件
hydrogenchloride in 1,4-dioxane T=50°C; 1.5 h;
参考文献
Synthesis, , # 4 p. 256 - 261
反应条件
ammonia in water Conversion of starting material;
参考文献
EP883597 B1, ;
Page/Page column 4-5 ;
反应条件
diethyl ether; aluminium amalgam; water
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 57, p. 13,22,1410
反应条件
T=100°C; P=250073 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 3121
