3-异丙基-4-甲基-1-炔基-3-戊醇合成路线 (共 18 条)
反应条件
in tetrahydrofuran
T=0 - 20°C;
参考文献
Yao, Gang; Haque, Serajul; Sha, Li; Kumaravel, Gnanasambandam; Wang, Joy; Engber, Thomas M.; Whalley, Eric T.; Conlon, Patrick R.; Chang, Hexi; Kiesman, William F.; Petter, Russell C.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 3 p. 511 - 515
反应条件
in tetrahydrofuran
Heating;
参考文献
Garratt, Dennis G.; Beaulieu, Pierre L.; Morisset, Veronique M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 927 - 934
反应条件
1: aqueous sulfuric acid; mercury (II)-sulfate
2: diethyl ether
3: sulfuric acid
4: lithium alanate
View Scheme
参考文献
Hickinbottom et al.
Journal of the Chemical Society, 1954 , p. 2529,2531
反应条件
trifluoroacetic acid; [Ru(η3-2-C3H4Me)(CO)(1,1'-(Ph2P)2-ferrocene)][SbF6] in tetrahydrofuran
T=60°C; Title compound not separated from byproducts;
参考文献
Cadierno, Victorio; Garcia-Garrido, Sergio E.; Gimeno, Jose
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 1-2 p. 101 - 110
反应条件
porcelain
T=300 - 320°C;
参考文献
Mesnard,D.; Miginiac,L.
Journal of Organometallic Chemistry, 1976 , vol. 117, p. 99 - 115
反应条件
pyridine; thionyl chloride
参考文献
Bhatia et al.
Journal of the Chemical Society, 1959 , p. 24,28
反应条件
T=300 - 320°C; Leiten ueber ungebranntes Porzellan;
参考文献
Faworskaja et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1490,1494;engl.Ausg.S.1564,1567
参考文献
Bhatia et al.
Journal of the Chemical Society, 1959 , p. 24,28