1-(2-硝基苯氧基)乙酮合成路线 （共 13 条）
反应条件
sodium hydrogencarbonate; tri-n-butylmethylammonium chloride; sodium bromide in water; toluene T=65°C; 6 h; Industry scaleInert atmosphere;
参考文献
US2010/222578 A1, ;
Page/Page column 3 ;
反应条件
potassium carbonate in water; N,N-dimethyl-formamide
反应条件
1: With ozone in methanol T=-78°C; 2: With dimethylsulfide; toluene-4-sulfonic acid in methanol T=-78 - 20°C; 4 h; 3: With amberlyst-15 in acetone T=20°C; 12 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 40, # 6 p. 1031 - 1039
反应条件
hydrogenchloride; sodium bromide; sodium hydrogencarbonate; sodium chloride in water; toluene
反应条件
potassium carbonate in acetone T=20°C; 16 h;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 14 p. 6608 - 6623
反应条件
Amberlite IRA-400(Cl(1-)) resin 8 h; 1.) H2O; 2.) acetone;
参考文献
Acta Chimica Hungarica, , vol. 124, # 3 p. 411 - 412
反应条件
acetone T=90°C; Erhitzen dann auf 115-120grad;
参考文献
Chemische Berichte, , vol. 30, p. 1635
DE97242 ;
反应条件
acetone; sodium iodide
参考文献
Journal of Organic Chemistry, , vol. 7, p. 251,257
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 7, p. 342 - 344
Zhurnal Organicheskoi Khimii, , vol. 7, # 2 p. 348 - 350
反应条件
hydrogen; sodium hydroxide; Amperkat SK Ni-Mo 3706 from HC Starck in methanol; toluene T=40°C; P=165017 Torr; pH=8 - 9; 1 h; Autoclave; Product distribution / selectivity;
参考文献
SALTIGO GMBH
Patent: US2011/40089 A1, 2011 ;
Location in patent: Page/Page column 5 ;
