1: With sodium hydride in diethyl ether; N,N-dimethyl-formamide 2: With n-butyllithium; boric acid trimethyl ester in tetrahydrofuran 3: With dihydrogen peroxide; acetic acid in tetrahydrofuran
参考文献
Centre National de la Recherche Scientifique (CNRS)
Patent: EP1792904 A1, 2007 ;
Location in patent: Page/Page column 17 ;
pinacol borane; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran byproducts: H2; C7H5O2OH reacted with (C2H5)2SiH2 and Ir complex in C6H6, reacted with Bcompds., Ir complex and 4,4'-di-tert-butylpyridine in THF at 80° C, reacted with aq. KHF2 in THF; obtained contaminated;
参考文献
Boebel, Timothy A.; Hartwig, John F.
Journal of the American Chemical Society, 2008 , vol. 130, # 24 p. 7534 - 7535