1,2,3,4,5,6,7,8-八氢菲合成路线 （共 80 条）
反应条件
hydrogen; nickel in water; ethylene glycol T=80°C; 0.1M NaCl, 0.05M H3BO3, pH 2.7 to 10.4; also in different solvents with various supporting electrolytes, at various temperatures and current densities; influence of pH and buffer; Product distribution;
参考文献
Canadian Journal of Chemistry, , vol. 68, # 7 p. 1218 - 1227
反应条件
hydrogen; tetra-n-propyl-diborane T=200°C; P=67505.4 Torr; 2 h; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 4 p. 719 - 724
反应条件
hydrogen; tetra-n-propyl-diborane T=200°C; P=67505.4 Torr; 10 h; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 4 p. 719 - 724
反应条件
1: NaBH4 / methanol 2: HCl-AcOH 3: 44 percent Spectr. / H2 / Pd/C / diethyl ether / 24 h / 25 °C View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 27, # 8 p. 796 - 797
反应条件
1: HCl-AcOH 2: 44 percent Spectr. / H2 / Pd/C / diethyl ether / 24 h / 25 °C View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 27, # 8 p. 796 - 797
反应条件
1: SnCl4 / benzene 2: NaBH4 / methanol 3: HCl-AcOH 4: 44 percent Spectr. / H2 / Pd/C / diethyl ether / 24 h / 25 °C View Scheme
参考文献
Magnetic Resonance in Chemistry, , vol. 27, # 8 p. 796 - 797
反应条件
aluminium trichloride T=50 - 70°C;
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 35, p. 631
DE333158 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 13, p. 380
Chemische Berichte, , vol. 57, p. 2014
Chem. Zentralbl., , vol. 99, # II p. 1386
反应条件
aluminium trichloride T=50 - 70°C; 7 h; Further byproducts given;
参考文献
Australian Journal of Chemistry, , vol. 37, # 11 p. 2379 - 2383
反应条件
hydrogen; nickel in water; ethylene glycol T=80°C; 0.1M NaCl, 0.1M H3BO3, pH 2.6-2.7 to 6.0-6.4; Product distribution;
参考文献
Robin, Denis; Comtois, Michel; Martel, Anna; Lemieux, Rene; Cheong, Amoy Kam; et al.
Canadian Journal of Chemistry, 1990 , vol. 68, # 7 p. 1218 - 1227
反应条件
phosphorus pentoxide T=320°C;
参考文献
Doklady Akademii Nauk SSSR, , vol. 99, p. 789,791
Chem.Abstr., , p. 5414
