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| CAS号 : | 573-17-1 |
精确质量 : | 255.98900 |
| 分子式 : | C14H9Br |
logP : | 4.75550 |
| 分子量 : | 257.12500 |
PSA : | 0.00000 |
9-溴菲 | |
9-Bromophenanthrene | |
573-17-1 | |
C14H9Br | |
257.12500 | |
0.00000 | |
4.75550 | |
255.98900 |
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1.6799 (100.7ºC)
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黄色晶体粉末
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>230 °F
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180-190 °C2 mm Hg(lit.)
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60-64 °C(lit.)
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1.479g/cm3
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Stable under normal temperatures and pressures.
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Store in a cool, dry place. Store in a tightly closed container.
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SF7197000
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3
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29036990
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S22-S24/25
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Xn; Xi
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R20/21/22
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2933990090
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2933990090. 其他仅含氮杂原子的杂环化合物. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:6.5%. 普通关税:20.0% | |
2933990090. heterocyclic compounds with nitrogen hetero-atom(s) only. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0% |
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暂时无法加载合成路线,请稍后刷新重试 |
<p>将菲溶于干燥的四氯化碳,加热回流,滴加溴素,继续回流逸尽生成的溴化氢。反应液减压蒸除溶剂,继续减压蒸馏,收集177-190℃(0.16kPa)馏分,即为9-溴菲,产率90%-94%。</p> | |
<p>用于有机合成。</p> |