3-(苄氧基)苯-1,2-二醇合成路线 （共 7 条）
反应条件
1: 100 percent / K2CO3 / acetone / 1 h / Heating 2: 98 percent / H2 / 10percent Pd-C / acetic acid / 0.5 h View Scheme
参考文献
Dietl, F.; Gierer, G.; Merz, A.
Synthesis, 1985 , # 6/7 p. 626 - 631
反应条件
1: 100 percent / K2CO3 / acetone / 1 h / Heating 2: 98 percent / H2 / 10percent Pd-C / acetic acid / 0.5 h 3: 78 percent / K2(SO3)2NO, aq. NaOAc / benzene View Scheme
参考文献
Dietl, F.; Gierer, G.; Merz, A.
Synthesis, 1985 , # 6/7 p. 626 - 631
反应条件
water; toluene-4-sulfonic acid in methanol
8 h; Ambient temperature; Yield given;
参考文献
Dietl, F.; Gierer, G.; Merz, A.
Synthesis, 1985 , # 6/7 p. 626 - 631
反应条件
1: 90 percent / NaOH / dioxane / 14 h / 100 °C
2: p-toluenesulfonic acid, H2O / methanol / 8 h / Ambient temperature
View Scheme
参考文献
Dietl, F.; Gierer, G.; Merz, A.
Synthesis, 1985 , # 6/7 p. 626 - 631
反应条件
1: 90 percent / NaOH / dioxane / 14 h / 100 °C
2: p-toluenesulfonic acid, H2O / methanol / 8 h / Ambient temperature
View Scheme
参考文献
Dietl, F.; Gierer, G.; Merz, A.
Synthesis, 1985 , # 6/7 p. 626 - 631
反应条件
1: 77 percent / ion-exchange resin Amberlyst 15 / benzene / 10 h / Heating
2: 90 percent / NaOH / dioxane / 14 h / 100 °C
3: p-toluenesulfonic acid, H2O / methanol / 8 h / Ambient temperature
View Scheme
参考文献
Dietl, F.; Gierer, G.; Merz, A.
Synthesis, 1985 , # 6/7 p. 626 - 631
反应条件
Na2B4O7; sodium hydroxide in water
10 h; Heating;
参考文献
Hayakawa, Kenji; Kido, Keiko; Kanematsu, Ken
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 511 - 520
