N-(2-苯基乙酰基)-甘氨酸甲酯合成路线 (共 10 条)
反应条件
1: 92 percent / POCl3 / 20 °C 2: 76 percent / EtONa / ethanol / 1 h / 20 °C View Scheme
参考文献
Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 9 p. 688 - 693
反应条件
ethanol; hydrazine hydrate
参考文献
Neher; Wettstein; Miescher
Helvetica Chimica Acta, 1946 , vol. 29, p. 1815,1824
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 12 h; Inert atmosphere;
参考文献
Pintori, Didier G.; Greaney, Michael F.
Organic Letters, 2011 , vol. 13, # 21 p. 5713 - 5715
反应条件
N-iodo-succinimide; water; potassium carbonate in tetrahydrofuran
T=0°C; 48 h;
参考文献
Shen, Bo; Makley, Dawn M.; Johnston, Jeffrey N.
Nature, 2010 , vol. 465, # 7301 p. 1027 - 1032
反应条件
in dichloromethane
18 h; Ambient temperature;
参考文献
Kumar, Arvind; Srivastava, Nivedita; Mital, Alka
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 6 p. 606 - 607
参考文献
Mloston; Romanski; Heimgartner
Polish Journal of Chemistry, 2001 , vol. 75, # 7 p. 975 - 982
反应条件
1: 95 percent / CH2Cl2 / 4 h
2: 65 percent / CH2Cl2 / 18 h / Ambient temperature
View Scheme
参考文献
Kumar, Arvind; Srivastava, Nivedita; Mital, Alka
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 6 p. 606 - 607
参考文献
Ose et al.
Yakugaku Zasshi, 1950 , vol. 70, p. 701
Chem.Abstr., 1951 , p. 6628
参考文献
Hurd; Prapas
Journal of Organic Chemistry, 1959 , vol. 24, p. 388,392
参考文献
Hotter
Journal fuer Praktische Chemie (Leipzig), 1888 , vol. <2> 38, p. 105