2-(2-氯氯苯基)-n-甲基乙胺合成路线 （共 10 条）
参考文献
Huisgen; Koenig
Chemische Berichte, 1959 , vol. 92, p. 203,211
反应条件
1: ammonium sulfate / 24 h / Heating
2: 64 percent / lithium diisopropylamide / pentane / -78 deg C to RT, overnight
View Scheme
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
参考文献
Huisgen; Koenig
Chemische Berichte, 1959 , vol. 92, p. 203,211
反应条件
borane-THF in tetrahydrofuran
Heating;
参考文献
Lewin, Anita H.; Navarro, Hernan A.; Wayne Mascarella
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 15 p. 7415 - 7423
反应条件
ammonium hydroxide; sodium hydroxide; sodium borohydride; iodine in tetrahydrofuran; methanol; tert-butyl methyl ether
参考文献
Andersen, Knud Erik; Dorwald, Florencio Zaragiza; Peschke, Bernd; Sidelmann, Ulla Grove; Rudolf, Klaus; Stenkamp, Dirk; Hurnaus, Rudolf; Muller, Stephan Georg; Krist, Bernd; Eriksen, Birgitte
Patent: US2002/58659 A1, 2002 ;
US 20020058659 A1
反应条件
1: dimethylformamide
2: LiAlH4, AlCl3
4: LiAlH4
View Scheme
参考文献
Jaques,B.; Wallace,R.G.
Tetrahedron, 1977 , vol. 33, p. 581 - 588
反应条件
lithium aluminium tetrahydride
24 h; Heating;
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
反应条件
2: LiAlH4 / 24 h / Heating
View Scheme
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
反应条件
2: LiAlH4; diethyl ether
View Scheme
参考文献
Huisgen; Koenig
Chemische Berichte, 1959 , vol. 92, p. 203,211
反应条件
1: LiAlH4, AlCl3
3: LiAlH4
View Scheme
参考文献
Jaques,B.; Wallace,R.G.
Tetrahedron, 1977 , vol. 33, p. 581 - 588
