1,2,4,5-四氟-3-碘苯合成路线 （共 12 条）
反应条件
(i) 2-prop-2-ynyloxy-tetrahydropyran <Cu(I) salt>, Py, (ii) H2SO4, MeOH; Multistep reaction;
参考文献
Barrow,I.; Pedler,A.E.
Tetrahedron, 1976 , vol. 32, p. 1829 - 1834
反应条件
phosphorous acid trisdiethylamide in hexane Dehalogenation; silyldeiodination; silyldeprotonation; 20 h;
参考文献
Bardin
Russian Chemical Bulletin, 1997 , vol. 46, # 4 p. 780 - 785
反应条件
phosphorous acid trisdiethylamide in hexane Dehalogenation; silyldeiodination; silyldeprotonation; 20 h;
参考文献
Russian Chemical Bulletin, , vol. 46, # 4 p. 780 - 785
反应条件
(i) CuI, aq. NH3, EtOH, (ii) /BRN= 2261072/, Py, (iii) H2SO4, MeOH; Multistep reaction;
参考文献
Barrow,I.; Pedler,A.E.
Tetrahedron, 1976 , vol. 32, p. 1829 - 1834
反应条件
(i) CuI, aq. NH3, EtOH, (ii) /BRN= 2261072/, Py, (iii) H2SO4, MeOH; Multistep reaction;
参考文献
Barrow,I.; Pedler,A.E.
Tetrahedron, 1976 , vol. 32, p. 1829 - 1834
反应条件
phosphorous acid trisdiethylamide in hexane
T=20°C; silyldeiodination; hydrodeiodination; 50 h;
参考文献
Bardin
Russian Chemical Bulletin, 1997 , vol. 46, # 4 p. 780 - 785
反应条件
sodium hydroxide; bromine
参考文献
Burdon,J. et al.
Tetrahedron, 1966 , vol. 22, p. 1183 - 1188
反应条件
water; phosphorous acid trisdiethylamide in N,N-dimethyl-formamide
T=20°C; protodeiodination; 0.333333 h;
参考文献
Bardin; Pressman
Russian Chemical Bulletin, 1997 , vol. 46, # 4 p. 786 - 788
反应条件
1: N2H4*H2O
2: Br2, aq. NaOH
View Scheme
参考文献
Burdon,J. et al.
Tetrahedron, 1966 , vol. 22, p. 1183 - 1188
参考文献
Birchall,J.M. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 2187 - 2191
