2-(2’-硝基-4’-氯苯偶氮)-4,6-二叔丁基酚合成路线 （共 7 条）
反应条件
1: 84 percent / glucose, 2N NaOH / ethanol / 1 h / Heating 2: 88 percent / Zn, 2N NaOH / ethanol / 1 h / Ambient temperature 3: 73 percent / Zn, 2N NaOH / ethanol / 5 h / Heating View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
反应条件
sodium hydroxide; thiourea dioxide in ethanol T=85 - 90°C; 1 h;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1984 , vol. 37, # 12 p. 2489 - 2497
反应条件
sodium hydroxide; TUD in water; isopropyl alcohol 3 h; Heating;
参考文献
Baik, Woonphil; Park, Tae Hong; Kim, Byeong Hyo; Jun, Young Moo
Journal of Organic Chemistry, 1995 , vol. 60, p. 5683 - 5685
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane 4 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane 4 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane
4 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
反应条件
hydrogenchloride; sodium lauryl sulfate
1.) diazotation, 2.) 45 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
