4,4'-[(E)-1,2-乙烯二基]二苯甲腈合成路线 （共 23 条）
反应条件
boric acid trimethyl ester; lithium tert-butylate in tetrahydrofuran; hexane 10 h; Heating;
参考文献
Kabalka, George W; Wu, Zhongzhi; Ju, Yuhong
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4759 - 4760
反应条件
1: 4-cyano-benzyl-phosphonic acid diethyl ester With sodium hydride in tetrahydrofuran T=20°C; Wadsworth-Emmons reaction; 0.5 h; Inert atmosphere; 2: [4-cyanophenyl]methanone in tetrahydrofuran T=65°C; Wadsworth-Emmons reaction; Inert atmosphere;
参考文献
Yao, Yishan; Shen, Wenting; Nohra, Brigitte; Lescop, Christophe; Reau, Regis
Chemistry - A European Journal, 2010 , vol. 16, # 24 p. 7143 - 7163
反应条件
1: ethanol; hydrazine hydrate 2: >120 View Scheme
参考文献
Fu; Sah
Journal of the American Chemical Society, 1942 , vol. 64, p. 1482
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Barber; Slack
Journal of the American Chemical Society, 1943 , vol. 65, p. 1776
反应条件
iodine; lithium hexamethyldisilazane 1.) THF, 2.) CCl4, reflux, irrad., 24 h; Multistep reaction;
参考文献
He, Gong-Xin; Mei, Houng-Yau; Bruice, Thomas C.
Journal of the American Chemical Society, 1991 , vol. 113, # 15 p. 5644 - 5650
参考文献
Bance; Barber; Woolman
Journal of the Chemical Society, 1943 , p. 1,3
参考文献
Bance; Barber; Woolman
Journal of the Chemical Society, 1943 , p. 1,3
反应条件
pyridine T=200 - 210°C;
参考文献
Bance; Barber; Woolman
Journal of the Chemical Society, 1943 , p. 1,3
反应条件
iodine; nitrobenzene
参考文献
Muizebelt,W.J.; Nivard,R.J.F.
Journal of the Chemical Society [Section] B: Physical Organic, 1968 , p. 913 - 920
反应条件
1: glacial acetic acid; bromine 2: pyridine / 200 °C View Scheme
参考文献
Bance; Barber; Woolman
Journal of the Chemical Society, 1943 , p. 1,3
反应条件
1: aqueous acetic acid; bromine 2: pyridine / 200 °C View Scheme
参考文献
Bance; Barber; Woolman
Journal of the Chemical Society, 1943 , p. 1,3
