3-(1-苯基乙基)-2,4-戊二酮合成路线 (共 22 条)
反应条件
amberlyst-15 in 1,2-dichloro-ethane
T=80°C; 0.25 h;
参考文献
Das, Biswanath; Krishnaiah, Martha; Laxminarayana, Keetha; Damodar, Kongara; Kumar, D. Nandan
Chemistry Letters, 2009 , vol. 38, # 1 p. 42 - 43
反应条件
ytterbium(III) triflate in nitromethane
T=100°C; 18 h;
参考文献
Liu, Jinqian; Wang, Limin; Zheng, Xingzhou; Wang, Aili; Zhu, Mengyun; Yu, Jianjun; Shen, Qiang
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1843 - 1846
反应条件
iodine in nitromethane
T=80°C; 1 h; Reactivity; SolventTime;
参考文献
Li, Zhongxian; Duan, Zheng; Wang, Huaiqiu; Tian, Rongqiang; Zhu, Qianrui; Wu, Yangjie
Synlett, 2008 , # 16 p. 2535 - 2539
反应条件
P(MeNCH2CH2)3N in hexane; acetonitrile
T=25°C; 0.5 h;
参考文献
Arumugam, Subramaniam; McLeod, Dale; Verkade, John G.
Journal of Organic Chemistry, 1998 , vol. 63, # 11 p. 3677 - 3679
反应条件
trifluorormethanesulfonic acid
T=100°C;
参考文献
Sanz, Roberto; Miguel, Delia; Martinez, Alberto; Alvarez-Gutierrez, Julia M.; Rodriguez, Felix
Organic Letters, 2007 , vol. 9, # 10 p. 2027 - 2030
反应条件
1: ethylbenzene With tertiary butyl peroxybenzenoate; bathophenanthroline; Cu(II) perchlorate
T=60°C; 6 h;
2: acetylacetone T=60°C; 22 h; Further stages.;
参考文献
Borduas, Nadine; Powell, David A.
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7822 - 7825
反应条件
cobalt(II) 2,4-pentanedionate in chloroform
T=80°C; 1 h;
参考文献
Vallribera, Adelina; Marquet, Jorge; Moreno-Manas, Marcial; Cayon, Eduard
Tetrahedron, 1993 , vol. 49, # 29 p. 6437 - 6450
反应条件
toluene-4-sulfonic acid in dichloromethane
Heating;
参考文献
Sanz, Roberto; Martinez, Alberto; Miguel, Delia; Alvarez-Gutierrez, Julia M.; Rodriguez, Felix
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 14 p. 1841 - 1845
反应条件
in chloroform
T=120°C; 0.1 h;
参考文献
Marquet, J.; Moreno-Manas, M.; Pacheco, P.; Vallribera, A.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1465 - 1468
反应条件
1-butyl-3-(3-sulfopropyl)-1H-imidazol-3-ium trifluoromethanesulfonate
T=100°C; 3 h; Ionic liquidInert atmosphere;
参考文献
Funabiki, Kazumasa; Komeda, Takuya; Kubota, Yasuhiro; Matsui, Masaki
Tetrahedron, 2009 , vol. 65, # 36 p. 7457 - 7463