1-氯-3-(2-氯乙基)-苯合成路线 （共 15 条）
反应条件
aluminium trichloride
参考文献
Ichii,M.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, # 9 p. 2810 - 2813
反应条件
1: With methanesulfonyl chloride; triethylamine in toluene
T=0°C; 1 h;
2: With lithium chloride in N,N-dimethyl-formamide
T=20°C; 24 h;
参考文献
Yus, Miguel; Ramon, Diego J.; Gomez, Inmaculada
Journal of Organometallic Chemistry, 2002 , vol. 663, # 1-2 p. 21 - 31
反应条件
tetraethylammonium chloride in acetonitrile
Heating;
参考文献
Hayami,J. et al.
Bulletin of the Chemical Society of Japan, 1971 , vol. 44, # 11 p. 3091 - 3095
反应条件
in hexane
T=-40°C; 1.5 h;
参考文献
Molchanov, A. P.; Vorob'eva, I. S.; Koroleva, L. B.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12 p. 2186 - 2189
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2523 - 2527
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
参考文献
Makosza,M.; Gajos,I.
Roczniki Chemii, 1974 , vol. 48, p. 1883 - 1893
反应条件
T=180 - 190°C; var. cyclopropanespiro-6-(4,4-dihalogenotetracyclo<6.2.1.02,7.03,5>undec-9-ene)-11-spirocyclopropanes; Mechanism;
参考文献
Molchanov, A. P.; Pecheritsyna, Ya. P.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 6.1 p. 1076 - 1081
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 6 p. 1195 - 1200
反应条件
potassium tert-butylate
1.) hexane, -40 deg C, 1.5 h, 2.) hexane, -40 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Molchanov, A. P.; Vorob'eva, I. S.; Koroleva, L. B.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12 p. 2186 - 2189
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2523 - 2527
反应条件
potassium tert-butylate
1.) hexane, -40 deg C, 1.5 h, 2.) hexane, -40 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Molchanov, A. P.; Vorob'eva, I. S.; Koroleva, L. B.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12 p. 2186 - 2189
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2523 - 2527
反应条件
potassium tert-butylate
1.) hexane, -40 deg C, 1.5 h, 2.) hexane, -40 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Molchanov, A. P.; Vorob'eva, I. S.; Koroleva, L. B.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12 p. 2186 - 2189
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2523 - 2527
反应条件
potassium tert-butylate
1.) hexane, -40 deg C, 1.5 h, 2.) hexane, -40 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Molchanov, A. P.; Vorob'eva, I. S.; Koroleva, L. B.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12 p. 2186 - 2189
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2523 - 2527
