1-氯-4-(苯基乙炔基)苯合成路线 （共 58 条）
反应条件
lanthanum; iodine in tetrahydrofuran
T=67°C; Fritsch-Buttenberg-Wiechell rearrangement; 3 h; Inert atmosphere;
参考文献
Umeda, Rui; Yuasa, Takumi; Anahara, Namika; Nishiyama, Yutaka
Journal of Organometallic Chemistry, 2011 , vol. 696, # 9 p. 1916 - 1919
反应条件
[(N-di(2-pyridyl)methyl-N'-cyclohexylurea)PdCl2]; tetra-n-butylammonium acetate in 1-methyl-pyrrolidin-2-one
T=110°C; Sonogashira-Hagihara reaction; 1 h;
参考文献
Najera, Carmen; Gil-Molto, Juan; Karlstroem, Sofia; Falvello, Larry R.
Organic Letters, 2003 , vol. 5, # 9 p. 1451 - 1454
反应条件
formic acid; 5-hydro-3-oxaoctafluoropentanesulfonyl fluoride; triethylamine; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=80°C; 18 h;
参考文献
Chen, Qing-Yun; He, Ya-Bo
Synthesis, 1988 , # 11 p. 896 - 897
反应条件
oxygen; bis(3-methoxysalicylidene)ethylenediaminatocobalt(II) in methanol; benzene
2 h; Ambient temperature;
参考文献
Inada, Akira; Nakamura, Yushin; Morita, Yutaka
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 3 p. 1041 - 1042
反应条件
bis-triphenylphosphine-palladium(II) chloride; oxygen in 1,4-dioxane
T=80°C; Sonogashira type coupling; 18 h;
参考文献
Wang, Xuan; Qin, Weiwei; Kakusawa, Naoki; Yasuike, Shuji; Kurita, Jyoji
Tetrahedron Letters, 2009 , vol. 50, # 46 p. 6293 - 6297
反应条件
[(N-di(2-pyridyl)methyl-N'-cyclohexylurea)PdCl2]; tetra-n-butylammonium acetate in 1-methyl-pyrrolidin-2-one
T=110°C; Sonogashira-Hagihara reaction; 2 h;
参考文献
Najera, Carmen; Gil-Molto, Juan; Karlstroem, Sofia; Falvello, Larry R.
Organic Letters, 2003 , vol. 5, # 9 p. 1451 - 1454
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide
T=20°C; 0.416667 h;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Doklady Chemistry, 1984 , vol. 274, p. 39 - 42
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 4 p. 818 - 822
反应条件
bis-(pyridin-2-yl)amine; Pd(NH3)2Cl2; triethylamine in water
T=25°C; Sonogashira Cross-Coupling; 6 h; Inert atmosphere;
参考文献
Zhong, Hong; Wang, Jinyun; Li, Liuyi; Wang, Ruihu
Dalton Transactions, 2014 , vol. 43, # 5 p. 2098 - 2103
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=85°C; 0.166667 h;
参考文献
Katritzky, Alan R.; Gordeev, Mikhail F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1295 - 1298
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile
T=20°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio; Cacchi, Sandro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4067 - 4070
