2-溴-4,5-二甲氧基苯乙腈合成路线 (共 8 条)
反应条件
1: NCS; PPh3; imidazole / CH2Cl2 / 8 h / 20 °C 2: 2.73 g / dimethylformamide / 6 h / 20 °C View Scheme
参考文献
Ito; Tanaka
Chemical and Pharmaceutical Bulletin, 1974 , vol. 22, # 9 p. 2108 - 2112
反应条件
bromine; sodium acetate; acetic acid
参考文献
Imbri, Dennis; Tauber, Johannes; Opatz, Till
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15080 - 15083
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 0.166667 h; Heating;
参考文献
Kyong, Dao Hung; Sladkov, V. I.; Suvorov, N. N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 9 p. 1732 - 1738
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 9 p. 1954 - 1961
参考文献
Molander, Gary A.; Pack, Shawn K.
Tetrahedron, 2003 , vol. 59, # 52 p. 10581 - 10591
参考文献
Ito; Tanaka
Chemical and Pharmaceutical Bulletin, 1974 , vol. 22, # 9 p. 2108 - 2112
反应条件
1: HCl / 80 °C 2: acetone; aqueous ethanol View Scheme
参考文献
Quelet
Bulletin de la Societe Chimique de France, 1953 , p. C 46
参考文献
Journal of the American Chemical Society, , vol. 59, p. 1541,1545
反应条件
ammonia; nickel
T=100°C; P=73550.8 Torr; Hydrogenation;
参考文献
Rumpf; Viel
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959 , vol. 249, p. 886