5-甲氧基-2,4-二硝基苯酚合成路线 （共 20 条）
反应条件
nitronium tetrafluoroborate in ethylene glycol dimethyl ether T=-50°C;
参考文献
Dwyer; Holzapfel
Tetrahedron, 1998 , vol. 54, # 27 p. 7843 - 7848
反应条件
ammonia; isopropylbenzene hydroperoxide in methanol; dichloromethane
参考文献
The Dow Chemical Company
Patent: US5414130 A1, 1995 ;
参考文献
The Dow Chemical Company
Patent: US5414130 A1, 1995 ;
参考文献
Borsche
Chemische Berichte, 1917 , vol. 50, p. 1354
反应条件
sodium hydroxide; sodium hypophosphite; alpha,alpha-dimethylbenzyl hydroperoxide 1.) CH2Cl2, liquid NH3, -33 deg C, 1 h, 2.) -10 deg C; room temperature, 4 h; Yield given. Multistep reaction;
参考文献
Pews, R. Garth; Lysrnko, Zenon; Vosejpka, Paul C.
Journal of Organic Chemistry, 1997 , vol. 62, # 23 p. 8255 - 8256
参考文献
Lock; Nottes
Monatshefte fuer Chemie, 1936 , vol. 68, p. 51,60
反应条件
1: nitric acid / -5 °C 2: aqueous KOH View Scheme
参考文献
Lock; Nottes
Monatshefte fuer Chemie, 1936 , vol. 68, p. 51,60
参考文献
Meldola; Eyre
P. Ch. S., p. 238
反应条件
1: nitric acid 2: aqueous alcoholic NaOH-solution View Scheme
参考文献
Blanksma
Recueil des Travaux Chimiques des Pays-Bas, 1904 , vol. 23, p. 122
Chem. Zentralbl., 1909 , vol. 80, # I p. 1809
反应条件
1: Diazotization.Eintragen des Reaktionsprodukts in alkoh. Natronlauge 2: fuming nitric acid View Scheme
参考文献
Meldola; Eyre
P. Ch. S., p. 238
