1-溴甲基-3-苯氧基苯合成路线 (共 19 条)
反应条件
1: 70 percent / Kolbe nitrile synthese 2: 90 percent / conc. H2SO4 / aq. acetic acid / 0.75 h / Heating View Scheme
参考文献
Matthies; Buchling
Archiv der Pharmazie, 1983 , vol. 316, # 7 p. 598 - 608
反应条件
in dimethyl sulfoxide T=20°C; 5 h;
参考文献
Dou, Dengfeng; Mandadapu, Sivakoteswara Rao; Alliston, Kevin R.; Kim, Yunjeong; Chang, Kyeong-Ok; Groutas, William C.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 19 p. 5749 - 5755
反应条件
potassium carbonate; 18-C-6 AN in acetonitrile 5 h; Heating;
参考文献
Shapiro, E. A.; Pereverzeva, Yu. O.; Nefedov, A. O.; Eismont, M. Yu.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 11.2 p. 2432 - 2433
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 11 p. 2647 - 2648
反应条件
dibenzo-18-crown-6 in acetonitrile 6 h; Heating;
参考文献
Shapiro, E. A.; Eismont, M. Yu.; Pereverzeva, Yu. O.; Nefedov, A. O.; Srashnenko, A. V.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.2 p. 573 - 577
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 652 - 656
反应条件
Kolbe nitrile synthese;
参考文献
Matthies; Buchling
Archiv der Pharmazie, 1983 , vol. 316, # 7 p. 598 - 608
反应条件
hydrogen in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; ethanol
参考文献
Zoecon Corporation
Patent: US4243819 A1, 1981 ;
反应条件
potassium hydroxide; tetra-(n-butyl)ammonium iodide in tetrahydrofuran 0.583333 h; Irradiation;
参考文献
Galin, F. Z.; Rakhimov, R. G.; Tolstikov, G. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.2 p. 170
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 168 p. 202 - 203
反应条件
potassium hydroxide; tetra-(n-butyl)ammonium iodide in tetrahydrofuran 8 h;
参考文献
Galin; Rakhimov; Vyrypaev; Bogdanov; Amirkhanov; Furlei; Tolstikov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 6 p. 826 - 835
参考文献
Zoecon Corporation
Patent: US4243819 A1, 1981 ;
反应条件
triethylamine in acetone T=35°C; 3 h;
参考文献
Badanyan; Stepanyan; Mikaelyan; Ovivyan; Panosyan
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 1 p. 34 - 41