2,2,4-三甲基-3-戊醇合成路线 (共 38 条)
反应条件
in diethyl ether; pentane
T=-10 - 20°C; 0.333333 h;
参考文献
Roberts, Donald D.; Hall, Edward W.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2573 - 2579
反应条件
lithium aluminium tetrahydride
参考文献
Foley et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2779,2280
参考文献
Conant; Blatt
Journal of the American Chemical Society, 1929 , vol. 51, p. 1233
Full Text Show Details
Faworski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1351
Chem. Zentralbl., 1913 , vol. 84, # I p. 1006
参考文献
Whitmore
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 566
Full Text Show Details
Greenwood; Whitmore; Crooks
Journal of the American Chemical Society, 1938 , vol. 60, p. 2028
反应条件
air; dihydrogen peroxide; Li2CuCl4 in acetonitrile
T=75°C; Product distribution; Further Variations:CatalystsReagentsTemperatures;
参考文献
Shul'Pin, Georgiy B.; Shilov, Alexander E.; Suess-Fink, Georg
Tetrahedron Letters, 2001 , vol. 42, # 41 p. 7253 - 7256
反应条件
1: copper / 250 - 300 °C
2: diethyl ether
View Scheme
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2789
Journal of the American Chemical Society, 1941 , vol. 63, p. 647
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
反应条件
magnesium in diethyl ether
参考文献
Bateman,L. et al.
Journal of the Chemical Society, 1962 , p. 3570 - 3578
反应条件
air; dihydrogen peroxide; olefin carbonyl osmium(0) in acetonitrile
T=60°C; Product distribution; Further Variations:CatalystsReagentsSolventsTemperatures;
参考文献
Shul'pin, Georgiy B.; Kudinov, Aleksandr R.; Shul'pina, Lidia S.; Petrovskaya, Elena A.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 5 p. 837 - 845