potassium carbonate in N,N-dimethyl-formamide
T=20°C;
参考文献
Lin, Yuya A.; Chalker, Justin M.; Floyd, Nicola; Bernardes, Goncalo J. L.; Davis, Benjamin G.
Journal of the American Chemical Society, 2008 , vol. 130, # 30 p. 9642 - 9643
1: 4-bromo-but-1-ene With magnesium in tetrahydrofuran
Inert atmosphere;
2: 2-methoxyacetonitrile in tetrahydrofuran
T=20°C; Inert atmosphereReflux;
3: With water; ammonium chloride in tetrahydrofuran
Inert atmosphereSaturated solution;
参考文献
Reznichenko, Alexander L.; Hampel, Frank; Hultzsch, Kai C.
Chemistry - A European Journal, 2009 , vol. 15, # 46 p. 12819 - 12827
1: 4-bromo-but-1-ene With magnesium in tetrahydrofuran
T=23°C; 2 h;
2: phenylacetyl chloride With copper(l) iodide in tetrahydrofuran
T=-15 - 23°C; Further stages.;
参考文献
Zabawa, Thomas P.; Chemler, Sherry R.
Organic Letters, 2007 , vol. 9, # 10 p. 2035 - 2038
