5-(2-羟苯基)-1H-四唑合成路线 （共 7 条）
反应条件
sodium azide; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Patil, Umakant B.; Kumthekar, Kedar R.; Nagarkar, Jayashree M.
Tetrahedron Letters, 2012 , vol. 53, # 29 p. 3706 - 3709
反应条件
hydrogenchloride; sodium azide; water; triethyl amine hydrochloride in toluene T=95 - 99°C; 6 h;
参考文献
Toyo Kasei Kogyo Company Limited
Patent: US5744612 A1, 1998 ;
反应条件
sodium chloride in water; ethyl acetate; toluene
参考文献
Kwon, Heon-Yong; Maggiarosa, Nicola; Lee, Ki-Soo; Cho, Min-Seok; Park, Jong-Sang; Cho, Joon-Hee; Lee, Yong-Ho; Lee, Byung-Ryul; Kim, Seon-Kyoung; Hong, Dae-Sik
Patent: US2010/256315 A1, 2010 ;
反应条件
[bmim][N3]; hydroxylamine; copper diacetate in N,N-dimethyl-formamide T=120°C; 12 h;
参考文献
Heravi, Majid M.; Fazeli, Azadeh; Oskooie, Hossein A.; Beheshtiha, Yahya S.; Valizadeh, Hassan
Synlett, 2012 , vol. 23, # 20 p. 2927 - 2930
反应条件
T=650 - 710°C; P=1.5 - 2 Torr; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4462 - 4465
反应条件
T=650 - 710°C; P=1.5 - 2 Torr; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4462 - 4465
反应条件
T=650 - 710°C; P=1.5 - 2 Torr; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4462 - 4465
