trichlorophosphate in N,N-dimethyl-formamide T=110°C; 18 h;
参考文献
Lai, Long-Li; Lin, Pen-Yuan; Wang, Jy-Shih; Hwu, Jih Ru; Shiao, Min-Jen; Tsay, Shwu-Chen
Journal of Chemical Research - Part S, 1996 , # 4 p. 194 - 195
Lai, Long-Li; Lin, Pen-Yuan; Wang, Jy-Shih; Hwu, Jih Ru; Shiao, Min-Jen; Tsay, Shwu-Chen
Journal of Chemical Research - Part S, 1996 , # 4 p. 194 - 195
Lai, Long-Li; Lin, Pen-Yuan; Wang, Jy-Shih; Hwu, Jih Ru; Shiao, Min-Jen; Tsay, Shwu-Chen
Journal of Chemical Research - Part S, 1996 , # 4 p. 194 - 195
1: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=80 - 90°C; 3 h; Inert atmosphere; 2: With hydrogenchloride in water pH=Ca. 4 - 6;
1: 2-Bromo-6-chloropyridine With n-butyllithium in tetrahydrofuran T=-78°C; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; 3: 2,3-dimethylbutane-2,3-diol With acetic acid in tetrahydrofuran
参考文献
Bouillon, Alexandre; Lancelot, Jean-Charles; Santos, Jana Sopkova De Oliveira; Collot, Valerie; Bovy, Philipppe R.; Rault, Sylvain
Tetrahedron, 2003 , vol. 59, # 50 p. 10043 - 10049
