2-甲基-2-丙烯-1-醇合成路线 (共 240 条)
反应条件
triphenyl phosphite; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene T=100°C; Suzuki-Miyaura coupling; 1 h;
参考文献
Kayaki, Yoshihito; Koda, Takashi; Ikariya, Takao
European Journal of Organic Chemistry, 2004 , # 24 p. 4989 - 4993
反应条件
propionic acid 8 h; Reflux;
参考文献
Cai, Zhengxin; Yongpruksa, Nattawut; Harmata, Michael
Organic Letters, 2012 , vol. 14, # 7 p. 1661 - 1663
反应条件
1: T=170°C; P=130 Torr; Heating / reflux; 2: With potassium dihydrogenphosphate T=20°C; 1.5 h;
参考文献
PARHAMI, Farhad; KIM, Woo-Kyun
Patent: WO2008/82520 A2, 2008 ;
Location in patent: Page/Page column 40 ;
反应条件
sodium hydrogencarbonate; palladium diacetate in water T=60°C; 0.333333 h;
参考文献
Synthesis, , # 20 p. 3443 - 3452
反应条件
hydrogenchloride; tin(ll) chloride 1.) dioxane, reflux, 7 h, 2.) dioxane, reflux, overnight; Yield given. Multistep reaction;
参考文献
Barclay; Vinqvist; Mukai; Itoh; Morimoto
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7416 - 7420
反应条件
[PtCl2(η2:η2-cycloocta-1,5-diene)]; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=80°C; 4 h; Microwave irradiation;
参考文献
Yang, Shyh-Chyun; Hsu, Yi-Chun; Gan, Kim-Hong
Tetrahedron, 2006 , vol. 62, # 17 p. 3949 - 3958
反应条件
[Pt(triphenylphosphine)2Cl2]; tin(ll) chloride T=150°C; Yields of byproduct given;
参考文献
Tsuji, Yasushi; Takeuchi, Ryo; Ogawa, Hiroshi; Watanabe, Yoshihisa
Chemistry Letters, 1986 , p. 293 - 294
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C;
参考文献
Nagamitsu, Tohru; Takano, Daisuke; Seki, Miyuki; Arima, Shiho; Ohtawa, Masaki; Shiomi, Kazuro; Harigaya, Yoshihiro; Omura, Satoshi
Tetrahedron, 2008 , vol. 64, # 35 p. 8117 - 8127
反应条件
2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate in dichloromethane T=0 - 20°C;
参考文献
Kotturi, Santosh R.; Tan, Jason S.; Lear, Martin J.
Tetrahedron Letters, 2009 , vol. 50, # 37 p. 5267 - 5269
反应条件
manganese(IV) oxide; 4 A molecular sieve in dichloromethane 3 h; Heating;
参考文献
McAllister, Graeme D.; Oswald, Magalie F.; Paxton, Richard J.; Raw, Steven A.; Taylor, Richard J.K.
Tetrahedron, 2006 , vol. 62, # 28 p. 6681 - 6694