2,3-二溴-1-丙烯合成路线 （共 153 条）
反应条件
phosphorus tribromide in toluene T=0 - 50°C; 3.25 h; Product distribution / selectivity;
参考文献
Mero, Christopher L.; Elnagar, Hassan Y.; Herndon JR., Robert C.
Patent: US2004/44259 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
sodium hydroxide; 1-hexadecylpyridinium bromide T=130°C; 2 h;
参考文献
Chin-Hsien, Wang
Synthesis, 1982 , # 6 p. 494 - 496
反应条件
phosphorus tribromide in isopar C T=6 - 50°C; 3.71667 h; Product distribution / selectivity;
参考文献
Mero, Christopher L.; Elnagar, Hassan Y.; Herndon JR., Robert C.
Patent: US2004/44259 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
KO2 in N,N-dimethyl-formamide
参考文献
Dureja, Prem; Casida, John E.; Ruzo, Luis O.
Tetrahedron Letters, 1982 , vol. 23, # 48 p. 5003 - 5004
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate in acetonitrile
参考文献
Mostamandi, A.; Remizova, L.A.; Pavlenkova, A.L.; Favorskaya, I.A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 850 - 852
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 980 - 983
反应条件
acetic acid; 9-bromo-9-bora-bicyclo[3.3.1]nonane 1.) CH2Cl2, room temperature, 1 h; Yield given. Multistep reaction;
参考文献
Hara, Shoji; Dojo, Hidetaka; Takinami, Satoru; Suzuki, Akira
Tetrahedron Letters, 1983 , vol. 24, # 7 p. 731 - 734
参考文献
Tollens
Justus Liebigs Annalen der Chemie, 1870 , vol. 156, p. 168
参考文献
v.Braun; Kuehn; Weismantel
Justus Liebigs Annalen der Chemie, 1926 , vol. 449, p. 260
反应条件
triethylamine in tetrahydrofuran T=35°C; 16 h;
参考文献
Frontier Scientific, Inc.
Patent: US2012/41193 A1, 2012 ;
Location in patent: Page/Page column 19 ;
反应条件
in tetrahydrofuran T=100°C; 3 h; Yield given;
参考文献
Capella, Laura; Montevecchi, Pier Carlo; Navacchia, Maria Luisa
Journal of Organic Chemistry, 1995 , vol. 60, # 23 p. 7424 - 7432
