N-(2-硝基苯基)-1,2-乙二胺合成路线 （共 10 条）
反应条件
1: Et3N / tetrahydrofuran / 24 h / Heating 2: SnCl2*2H2O / dimethylformamide / 12 h / 60 °C 3: H+ / toluene / 1 h / 100 °C 4: Me2NH / methanol View Scheme
参考文献
Kennedy, Gordon; Viziano, Monica; Winders, John Alexander; Cavallini, Palmina; Gevi, Monica; Micheli, Fabrizio; Rodegher, Pamela; Seneci, Pierfausto; Zumerle, Aurelia
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 15 p. 1751 - 1754
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Singh, Ram; Geetanjali
Synthesis, 2005 , # 14 art. no. P04405SS, p. 2315 - 2320
参考文献
Boga, Carla; Forlani, Luciano; Guardia, Patrizia
Gazzetta Chimica Italiana, 1997 , vol. 127, # 5 p. 259 - 262
参考文献
Allali, Mustapha; Benoist, Eric; Habbadi, Nouzha; Gressier, Marie; Souizi, Abdelaziz; Dartiguenave, Michele
Tetrahedron, 2004 , vol. 60, # 5 p. 1167 - 1174
反应条件
trifluoroacetic acid in dichloromethane
acidolysis; Heating;
参考文献
Kennedy, Gordon; Viziano, Monica; Winders, John Alexander; Cavallini, Palmina; Gevi, Monica; Micheli, Fabrizio; Rodegher, Pamela; Seneci, Pierfausto; Zumerle, Aurelia
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 15 p. 1751 - 1754
参考文献
Singh, Ram; Geetanjali
Synthesis, 2005 , # 14 art. no. P04405SS, p. 2315 - 2320
参考文献
Fourneau; Lestrange
Bulletin de la Societe Chimique de France, 1947 , p. 827,829,831
反应条件
in toluene
T=25°C; also in DMSO; Rate constant;
参考文献
Boga, Carla; Forlani, Luciano; Guardia, Patrizia
Gazzetta Chimica Italiana, 1997 , vol. 127, # 5 p. 259 - 262
反应条件
potassium carbonate in water; acetone
T=20°C; 3 h;
参考文献
Wyeth
Patent: US2005/20575 A1, 2005 ;
Location in patent: Page/Page column 9 ;
US 20050020575 A1
反应条件
2: iron-powder; water; ethanol / Reagens 4: Salzsaeure
4: POCl3
5: ethanol; N2H4+H2O
View Scheme
参考文献
Foster et al.
Journal of the Chemical Society, 1957 , p. 1671,1673
