4-羟基-4-联苯基羧酸乙酯合成路线 （共 15 条）
反应条件
sulfuric acid in benzene 36 h; Heating;
参考文献
Busson; Oertegren; Ihre; Gedde; Hult; Andersson; Eriksson; Lindgren
Macromolecules, 2002 , vol. 35, # 5 p. 1663 - 1671
参考文献
He, Lingyan; Zhang, Liang; Liu, Xiaofeng; Li, Xianghua; Zheng, Mingyue; Li, HongLin; Yu, Kunqian; Chen, Kaixian; Shen, Xu; Jiang, Hualiang; Liu, Hong
Journal of Medicinal Chemistry, 2009 , vol. 52, # 8 p. 2465 - 2481
反应条件
1: Br2, (CF3CO)2O / FeCl3 / CCl4 2: KOH / ethanol 3: K2CO3 / acetone 4: Mg, C2H5Br / diethyl ether 5: 48percent HBr / acetic acid 6: H(+) / toluene View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in benzene Suzuki coupling; RefluxDarknessInert atmosphere;
参考文献
Abdu-Allah, Hajjaj H. M.; Tamanaka, Taichi; Yu, Jie; Zhuoyuan, Lu; Sadagopan, Magesh; Adachi, Takahiro; Tsubata, Takeshi; Kelm, Soerge; Ishida, Hideharu; Kiso, Makoto
Journal of Medicinal Chemistry, 2008 , vol. 51, # 21 p. 6665 - 6681
反应条件
1: K2CO3 / acetone 2: Mg, C2H5Br / diethyl ether 3: 48percent HBr / acetic acid 4: H(+) / toluene View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
1: Mg, C2H5Br / diethyl ether 2: 48percent HBr / acetic acid 3: H(+) / toluene View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
1: 48percent HBr / acetic acid 2: H(+) / toluene View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
1: KOH / ethanol 2: K2CO3 / acetone 3: Mg, C2H5Br / diethyl ether 4: 48percent HBr / acetic acid 5: H(+) / toluene View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydroxide 1.) DMSO, 120 deg C, 1 h, 2.) DMSO, 70 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Lee, Myongsoo; Oh, Nam-Keun
Journal of Materials Chemistry, 1996 , vol. 6, # 7 p. 1079 - 1086
反应条件
1: K2CO3 / acetone / Heating 2: aq. NaOH / methanol / Heating View Scheme
参考文献
Srinivasan, Murugesan Vijay; Kannan, Palaninathan; Roy, Arun
New Journal of Chemistry, 2013 , vol. 37, # 5 p. 1584 - 1590
