1-[(4-甲基苯基)磺酰]-1H-吲哚-3-甲醛合成路线 （共 13 条）
反应条件
dibenzo-18-crown-6; potassium carbonate in dichloromethane 18 h; Heating;
参考文献
Cheskis, B. A.; Alekseev, I. G.; Moiseenkov, A. M.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 2.2 p. 364 - 369
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 2 p. 425 - 432
反应条件
Iron (III) nitrate nonahydrate; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; sodium chloride in toluene T=20°C; 6.5 h;
参考文献
Liu, Jinxian; Ma, Shengming
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 25 p. 4186 - 4193
反应条件
silver trifluoromethanesulfonate in dichloromethane T=-78 - 0°C; 0.666667 h; Inert atmosphere;
参考文献
Ohsawa, Kosuke; Yoshida, Masahito; Doi, Takayuki
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3438 - 3444
反应条件
1: 1H-indole-3-carbaldehyde With sodium hydride in acetonitrile 2: tosyl halide in acetonitrile
参考文献
Singh, Palwinder; Kaur, Matinder; Holzer, Wolfgang
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 11 p. 4968 - 4982
反应条件
1: trichlorophosphate / |Cooling with ice 2: |Alkaline conditions View Scheme
参考文献
Che, Zhiping; Zhang, Shaoyong; Shao, Yonghua; Fan, Lingling; Xu, Hui; Yu, Xiang; Zhi, Xiaoyan; Yao, Xiaojun; Zhang, Rui
Journal of Agricultural and Food Chemistry, 2013 , vol. 61, # 24 p. 5696 - 5705
反应条件
1: ethanol / Ambient temperature 2: 1percent aq. NaOH / ethanol View Scheme
参考文献
Moriya, Tamon; Hagio, Katsuaki; Yoneda, Naoto
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 6 p. 1711 - 1721
反应条件
lithium hydroxide; mercaptoacetic acid in N,N-dimethyl-formamide T=20°C; 1.5 h;
参考文献
Griffiths-Jones, Charlotte M.; Knight, David W.
Tetrahedron, 2011 , vol. 67, # 44 p. 8515 - 8528
反应条件
potassium carbonate in methanol 2 h; Heating;
参考文献
Chakrabarty, Manas; Basak, Ramkrishna; Harigaya, Yoshihiro; Takayanagi, Hiroaki
Tetrahedron, 2005 , vol. 61, # 7 p. 1793 - 1801
反应条件
1: 1.) butyllithium / 1.) ether, hexane, r.t., 2 h, 2.) THF, 15 h 2: CF3COOH / toluene / 2 h / Ambient temperature 3: 72 percent / 20percent aq. NaOH / ethanol / 2.5 h / Heating View Scheme
参考文献
Achenbach; Franke
Archiv der Pharmazie, 1987 , vol. 320, # 6 p. 574 - 576
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol; water
T=90°C; 0.333333 h;
参考文献
Kutschy, Peter; Dzurilla, Milan; Takasugi, Mitsuo; Toeroek, Marcel; Achbergerova, Ingrid; Homzova, Renata; Racova, Maria
Tetrahedron, 1998 , vol. 54, # 14 p. 3549 - 3566
