carbon monoxide in tetrahydrofuran byproducts: (p-Tol)2CO; High Pressure; 0.05 mmol Pd compound, 0.1 mmol (p-Tol)2Zn, 2.5 ml THF, CO 30 atm (at -50°), stirred at 25°C for 2 h in presence of 0.2 mmol MgClBr; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide; triethylamine in dichloromethane 35 atm CO, presence of Et3N, N2-atmosphere, stirring for 30 min at 60°C; GC-anal., product selectivity detd.;
参考文献
Journal of molecular catalysis, , vol. 48, # 1 p. 69 - 79
carbon monoxide in tetrahydrofuran byproducts: (p-Tol)2CO; High Pressure; 0.05 mmol Pd compound, 0.1 mmol (p-Tol)2Zn, 2.5 ml THF, CO 30 atm (at -50°), stirred at 25°C for 2 h in presence of 0.2 mmol MgClBr; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide; triethylamine in acetonitrile 10 atm CO, presence of Et3N, N2-atmosphere, mixing at -20°C, stirring for 1 h at 40°C; GC-anal., product selectivity detd.;
参考文献
Yamashita; Sakakura; Kobayashi; Tanaka
Journal of molecular catalysis, 1988 , vol. 48, # 1 p. 69 - 79
