carbon monoxide in tetrahydrofuran High Pressure; 0.05 mmol Pd compound, 0.1 mmol Et2Hg, 2,5 ml THF, CO 30 atm (at -50°C), stirred for 2 h at 25°C in presence of 0.2 mmol MgClBr; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide in tetrahydrofuran High Pressure; 0.05 mmol Pd compound, 0.1 mmol EtZnCl, 2,5 ml THF, CO 30 atm (at -50°C), stirred for 2 h at 25°C in presence of 0.1 mmol MgClBr (yield of PhCEt(OH)COEt/PhCOCEt2(OH): 21percent); GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide in tetrahydrofuran; hexane High Pressure; 0.05 mmol Pd compound, 0.1 mmol Et3Al, 2,5 ml THF/hexane (24/1), CO 30 atm (at -50°C), stirred for 2 h at 25°C; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide; ethylmagnesium bromide in tetrahydrofuran High Pressure; 0.05 mmol Pd compound, 0.1 mmol EtMgBr, 2,5 ml THF, CO 30 atm (at -50°C), stirred for 2 h at 25°C; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide in tetrahydrofuran High Pressure; 0.05 mmol Pd compound, 0.1 mmol EtCu, 2,5 ml THF, CO 30 atm (at -50°C), stirred for 2 h at 25°C in presence of 0.1 mmol MgBrI (yield of PhCEt(OH)COEt/PhCOCEt2(OH): 17percent); GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide in tetrahydrofuran; hexane High Pressure; 0.05 mmol Pd compound, 0.1 mmol Et2AlCl, 2,5 ml THF/hexane (24/1), CO 30 atm (at -50°C), stirred for 2 h at 25°C; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide in tetrahydrofuran High Pressure; 0.05 mmol Pd compound, 0.1 mmol Et2Cd, 2,5 ml THF, CO 30 atm (at -50°C), stirred for 2 h at 25°C in presence of 0.2 mmol MgClBr (yield of PhCEt(OH)COEt/PhCOCEt2(OH): 71percent); GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
carbon monoxide in diethyl ether High Pressure; 0.05 mmol Pd compound, 0.1 mmol EtMnI, 2,5 ml Et2O, CO 30 atm (at -50°C), stirred for 2 h at 25°C in presence of 0.1 mmol MgBrI; GC-MS, GC;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 125 - 132
