(1Alpha,3Alpha,5Alpha)-1,3,5-环己三醇合成路线 （共 10 条）
反应条件
hydrogen; nickel in ethanol; water P=112509 - 150012 Torr; 48 h; Ambient temperature;
参考文献
Stetter, Hermann; Hunds, Artur
Liebigs Annalen der Chemie, 1984 , # 9 p. 1577 - 1590
反应条件
nickel-cobalt-copper catalyst; decalin T=100 - 125°C; P=44130.5 Torr; Hydrogenation;
参考文献
Stetter; Steinacker
Chemische Berichte, 1952 , vol. 85, p. 451,453
反应条件
T=100 - 125°C; P=36775.4 Torr; Hydrogenation;
参考文献
Lindemann; Baumann
Justus Liebigs Annalen der Chemie, 1930 , vol. 477, p. 78,90
反应条件
T=100 - 125°C; P=36775.4 Torr; Hydrogenation;
参考文献
Lindemann; Baumann
Justus Liebigs Annalen der Chemie, 1930 , vol. 477, p. 78,90
反应条件
T=100 - 125°C; P=36775.4 Torr; Hydrogenation;
参考文献
Lindemann; Baumann
Justus Liebigs Annalen der Chemie, 1930 , vol. 477, p. 78,90
反应条件
boron trifluoride Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Laatsch, Hartmut; Pudleiner, Alke
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 8 p. 663 - 677
反应条件
hydrogenchloride; methanol
参考文献
Bouab, Otmane; Lamaty, Gerard; Moreau, Claude; Pomares, Odile; Deslongchamps, Pierre; Ruest, Luc
Canadian Journal of Chemistry, 1980 , vol. 58, p. 567 - 573
参考文献
Stetter; Steinacker
Chemische Berichte, 1953 , vol. 86, p. 790,793
反应条件
hydrogenchloride; methanol
参考文献
Stetter; Steinacker
Chemische Berichte, 1953 , vol. 86, p. 790,793
反应条件
1: 91 percent / Et2O*BF3 / CH2Cl2 / 1.) 8 - 12 h, reflux; 2.) 24 h at room temp.
2: 96 percent / 2N KOH / ethanol / 1.) a few minutes heating to reflux; 2.) 0 deg C
3: SOCl2 / 0.5 h / Heating
View Scheme
参考文献
Stetter, Hermann; Hunds, Artur
Liebigs Annalen der Chemie, 1984 , # 9 p. 1577 - 1590
