2-乙基-1H-异吲哚-1,3(2H)-二酮合成路线 (共 56 条)
反应条件
benzophenone; oxygen in tert-butyl alcohol T=30°C; 23 h; Irradiation;
参考文献
Gramain, J. C.; Simonet, N.; Vermeersch, G.; Febvay-Garot, N.; Caplain, S.; Lablache-Combier, A.
Tetrahedron, 1982 , vol. 38, # 4 p. 539 - 550
反应条件
potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate in 1,1-dimethylpropan-1-ol T=100°C; P=760.051 Torr; 24 h;
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
PhP(C6H4-p-(CH2)2C6F13)2; diethylazodicarboxylate in tetrahydrofuran
参考文献
Dandapani, Sivaraman; Curran, Dennis P.
Tetrahedron, 2002 , vol. 58, # 20 p. 3855 - 3864
反应条件
acrylic acid methyl ester in acetonitrile 8 h; Irradiation; Further byproducts given;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
反应条件
thionyl chloride Erhitzen des Reaktionsprodukts auf 250grad/1-2 Torr;
参考文献
Mayer, Klaus K.; Poettinger, Theodor; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1981 , vol. 314, # 8 p. 669 - 674
反应条件
in acetonitrile 8 h; Irradiation; Further byproducts given;
参考文献
Yoon, Ung Chan; Kim, Dong Uk; Lee, Chan Woo; Choi, Young Sun; Lee, Yean-Jang; Ammon, Herman L.; Mariano, Patrick S.
Journal of the American Chemical Society, 1995 , vol. 117, # 10 p. 2698 - 2710
参考文献
White; Morrison; Anderson
Journal of the American Chemical Society, 1924 , vol. 46, p. 967
反应条件
quinoline; hydrogen; Pd-BaSO4 in xylene Heating; Yield given;
参考文献
Mayer, Klaus K.; Poettinger, Theodor; Wiegrebe, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1981 , vol. 314, # 8 p. 669 - 674
反应条件
potassium carbonate in water; acetone T=20°C; 12 h; Irradiation; Title compound not separated from byproducts;
参考文献
Griesbeck, Axel G.; Henz, Andreas; Peters, Karl; Peters, Eva-Maria; Schnering, Hans Georg von
Angewandte Chemie, 1995 , vol. 107, # 4 p. 498 - 500
反应条件
30 min, 110 deg C; 1 h, 130 deg C; 3 h, 180 deg C;
参考文献
Kreher, Richard P.; Hennige, Hans; Jelitto, Frank; Preut, Johannes
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 9 p. 1132 - 1148