1-羟基-3-苯基-丙-2-酮合成路线 (共 25 条)
反应条件
gold(III) chloride; silver hexafluoroantimonate in 1,4-dioxane
T=20°C; 0.166667 h; regioselective reaction;
参考文献
Gudla, Vanajakshi; Balamurugan, Rengarajan
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5243 - 5247
反应条件
zeolite H-Y in dichloromethane
T=20°C; 4 h;
参考文献
Muthusamy, Sengodagounder; Babu, Srinivasarao Arulananda; Gunanathan, Chidambaram; Jasra, Raksh Vir
Synlett, 2002 , # 3 p. 407 - 410
反应条件
1: With titanium tetrachloride
T=20°C; silylation; 3 h;
2: With hydrogenchloride in 1,4-dioxane
T=90°C; Hydrolysis; 0.166667 h; Further stages.;
参考文献
Liu; Xu; Szalkowski; Li; Ding; Kwei; Huskey; Moller; Heck; Zhang; Jones
Journal of Medicinal Chemistry, 2000 , vol. 43, # 19 p. 3487 - 3494
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=-100 - 0°C;
参考文献
Dalla; Catteau
Tetrahedron, 1999 , vol. 55, # 21 p. 6497 - 6510
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=-100 - 20°C;
参考文献
Dalla; Catteau
Tetrahedron, 1999 , vol. 55, # 21 p. 6497 - 6510
反应条件
lithium aluminium tetrahydride in diethyl ether
T=-100 - -15°C; Yields of byproduct given;
参考文献
Dalla; Catteau
Tetrahedron, 1999 , vol. 55, # 21 p. 6497 - 6510
反应条件
peracetic acid; osmium(III) chloride in various solvent(s)
3 h; Ambient temperatureother alkenes; Mechanism;
参考文献
Murahashi, Sun-Ichi; Naota, Takeshi; Hanaoka, Hidenori
Chemistry Letters, 1993 , # 10 p. 1767 - 1770
反应条件
lithium boron tetrafluoride in dichloromethane; acetonitrile
15 h; Ambient temperature;
参考文献
Ferraboschi, Patrizia; Grisenti, Paride; Manzocchi, Ada; Santaniello, Enzo
Tetrahedron, 1994 , vol. 50, # 35 p. 10539 - 10548
反应条件
titanium tetrachloride in dichloromethane
T=-78 - 20°C; 5 h;
参考文献
Hon, Yung-Son; Devulapally, Rammohan
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2831 - 2834
反应条件
lithium aluminium tetrahydride in diethyl ether
T=-100 - -20°C; Yields of byproduct given;
参考文献
Dalla; Catteau
Tetrahedron, 1999 , vol. 55, # 21 p. 6497 - 6510