1,6-脱水-β-D-葡萄糖合成路线 （共 127 条）
反应条件
scandium tris(trifluoromethanesulfonate) T=20°C; 0.2 h;
参考文献
Lee, Jinq-Chyi; Tai, Cheng-An; Hung, Shang-Cheng
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 851 - 855
反应条件
pyridine T=0°C; 1.5 h;
参考文献
Carbohydrate Research, , vol. 108, p. 71 - 80
反应条件
CRL 264 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Boissiere-Junot, Nathalie; Tellier, Charles; Rabiller, Claude
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 1 p. 99 - 115
反应条件
H-MCM-36-P22-28 zeolite T=299.84°C; P=760.051 Torr; Gas phase;
参考文献
Kaeldstroem; Kumar; Heikkilae; Murzin, D.Yu.
Applied Catalysis A: General, 2011 , vol. 397, # 1-2 p. 13 - 21
反应条件
hydrogenchloride; water; zinc(II) chloride T=70°C; 0.25 h;
参考文献
BIOECON INTERNATIONAL HOLDING N.V.; PETROLEO BRASILEIRO S.A. - PETROBRAS; TSCHENTSCHER, Roman; MENEGASSI DE ALMEIDA, Rafael; CARUCCI, José Rafael Hernández; VAN DEN BERGH, Johan; MOULIJN, Jacob Adriaan
Patent: WO2013/110814 A1, 2013 ;
Location in patent: Paragraph 00156 ;
反应条件
1.1: 1H-imidazole / tetrahydrofuran / 0 °C 2.1: magnesium / tetrahydrofuran; ethylene dibromide / |Reflux 2.2: 1 h / 20 °C 2.3: 8 h / 20 - 130 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C View Scheme
反应条件
scandium tris(trifluoromethanesulfonate) T=20°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 5 p. 851 - 855
反应条件
H-MCM-36-P22-28 zeolite T=299.84°C; P=760.051 Torr; Gas phase;
参考文献
Kaeldstroem; Kumar; Heikkilae; Murzin, D.Yu.
Applied Catalysis A: General, 2011 , vol. 397, # 1-2 p. 13 - 21
反应条件
Amberlyst 70 in water T=170°C; 3 h; AutoclaveInert atmosphere;
参考文献
Hu, Xun; Wu, Liping; Wang, Yi; Mourant, Daniel; Lievens, Caroline; Gunawan, Richard; Li, Chun-Zhu
Green Chemistry, 2012 , vol. 14, # 11 p. 3087 - 3098
反应条件
BaO in N,N-dimethyl-formamide T=60°C; Inert atmosphere; regioselective reaction;
参考文献
Zhu, Xiangming; Dere, Ravindra T.; Jiang, Junyan; Zhang, Lei; Wang, Xiaoxia
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10187 - 10197
