2,4,6-三异丙基苯甲酸合成路线 (共 21 条)
反应条件
1: LiAlH4 / diethyl ether 2: thionyl chloride View Scheme
参考文献
Wagner, Peter J.; Meador, Michael A.; Zhou, Boli; Park, Bong-Ser
Journal of the American Chemical Society, 1991 , vol. 113, # 25 p. 9630 - 9639
反应条件
1: thionyl chloride / Reflux 2: diethyl ether; toluene / 24 h / 0 °C / Inert atmosphere View Scheme
参考文献
Zhang, Jian; Yang, Nianfa; Yang, Liwen
Molecules, 2012 , vol. 17, # 6 p. 6415 - 6423
参考文献
Beak, Peter; Becker, Peter D.
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3855 - 3861
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in chloroform; water 16 h; Ambient temperature;
参考文献
Chen, Jack L.-Y.; Scott, Helen K.; Hesse, Matthew J.; Willis, Christine L.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2013 , vol. 135, # 14 p. 5316 - 5319
反应条件
1-n-butyl-3-methylimidazolium hexafluorophosphate T=80°C; 3 h;
参考文献
Yoshino, Tomonori; Imori, Satomi; Togo, Hideo
Tetrahedron, 2006 , vol. 62, # 6 p. 1309 - 1317
反应条件
sulfuric acid in toluene 24 h; Reflux;
参考文献
Martin, Veronique; Blakey, Simon
Tetrahedron Letters, 2008 , vol. 49, # 48 p. 6800 - 6803
反应条件
1: thionyl chloride / 16 h / Heating 2: pyridine / 21 h / Heating View Scheme
参考文献
Beak, Peter; Carter, Linda G.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2363 - 2373
反应条件
1: thionyl chloride / 12 h / Heating
2: diethyl ether / 3 h
View Scheme
参考文献
Beak, Peter; Zajdel, William J.
Journal of the American Chemical Society, 1984 , vol. 106, # 4 p. 1010 - 1018
反应条件
1: thionyl chloride / 12 h / Heating
2: diethyl ether
View Scheme
参考文献
Beak, Peter; Zajdel, William J.
Journal of the American Chemical Society, 1984 , vol. 106, # 4 p. 1010 - 1018
反应条件
1: thionyl chloride / 12 h / Heating
2: diethyl ether
View Scheme
参考文献
Beak, Peter; Zajdel, William J.
Journal of the American Chemical Society, 1984 , vol. 106, # 4 p. 1010 - 1018