2-甲基-2-(磺基氧基)丙酰胺合成路线 （共 12 条）
反应条件
sulfuric acid in water Industry scale;
参考文献
Carlson JR., Curtis Ingstad; DeCourcy, Michael Stanley; Juliette, Jamie Jerrick John
Patent: US2003/208093 A1, 2003 ;
Location in patent: Page/Page column 3; Sheet 1 ;
反应条件
methanesulfonic acid; water T=130°C; P=1875.19 Torr; 1 h; Product distribution / selectivity;
参考文献
ROeHM GMBH and CO. KG
Patent: WO2005/77878 A1, 2005 ;
Location in patent: Page/Page column 29 ;
反应条件
water; acetic acid T=115°C; P=1875.19 Torr; 1 h; Product distribution / selectivity;
参考文献
WO2005/77878 A1, ;
Page/Page column 27 ;
反应条件
sulfuric acid Heating;
参考文献
Hall, C. Dennis; Leeding, Christopher J.; Jones, Stephen; Case-Green, Stephen; Sanderson, Ian; Hoorn, Marielle van
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 3 p. 417 - 422
反应条件
water T=74.9°C; Rate constant;
参考文献
Hall, C. Dennis; Leeding, Christopher J.; Jones, Stephen; Case-Green, Stephen; Sanderson, Ian; Hoorn, Marielle van
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 3 p. 417 - 422
反应条件
water; acetic acid T=115°C; P=1875.19 Torr; 1 h; Product distribution / selectivity;
参考文献
WO2005/77878 A1, ;
Page/Page column 27 ;
反应条件
sulfuric acid in nitromethane
T=5°C;
参考文献
Hall, C. Dennis; Leeding, Christopher J.; Jones, Stephen; Case-Green, Stephen; Sanderson, Ian; Hoorn, Marielle van
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 3 p. 417 - 422
反应条件
sulfuric acid
T=85 - 101°C; 0.666667 h; CSTR reactor; Product distribution / selectivity;
参考文献
Schladenhauffen, Paul Benjamin; DeCourcy, Michael Stanley; Chang-Mateu, I-Hwa Midey; Wilczynski, Robert; Zolotorofe, Donald
Patent: US2006/111586 A1, 2006 ;
Location in patent: Page/Page column 5-6; 8 ;
反应条件
nitromethane; sulfuric acid; water
T=40 - 55°C; 0.5 h; Product distribution / selectivity;
参考文献
ROeHM GMBH and CO. KG
Patent: WO2005/77878 A1, 2005 ;
Location in patent: Page/Page column 23-24 ;
反应条件
sulfuric acid; sulfur trioxide
参考文献
Michurin,A.A. et al.
J. Appl. Chem. USSR (Engl. Transl.), 1974 , vol. 47, # 6 p. 1347 - 1351,1383 - 1386
