Lipilin, Dmitriy L.; Churakov, Aleksandr M.; Ioffe, Sema L.; Strelenko, Yuri A.; Tartakovsky, Vladimir A.
European Journal of Organic Chemistry, 1999 , # 1 p. 29 - 35
in tetrahydrofuran Irradiation (UV/VIS); A soln. of nitroso compound in THF under N2 is stirred until it becomes light blue, to this soln. is added metal carbonyl, the soln. is irradiated (sunlamp photolysis) for a period of 1 h at 30°C.; reaction mixture is cooled to 25°C, the solvent is removed, purifn. by chromy. on silica gel using 19/1 hexane/ethyl acetate as eluent for the second fraction, first fraction is eluted with hexane;
参考文献
Herndon, James W.; McMullen, Leonard A.
Journal of Organometallic Chemistry, 1989 , vol. 368, p. 83 - 102
sodium tetraphenyl borate in tetrahydrofuran To a filtered soln. obtained from complex, NaBPh4 and THF was added nitrosobenzene in THF in 40 min, stirred for 2 h (N2 atm.);; filtered;;
参考文献
Fochi, Giovanni; Floriani, Carlo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 2577 - 2580
ruthenium trichloride; dihydrogen peroxide; N,N-didecyl-N,N-dimethylammonium bromide in 1,2-dichloro-ethane T=90°C; 24 h; var. phase-transfer catalysts, var. conc. of H2O2; Product distribution;
参考文献
Dodonov; Zaburdaeva; Stepovik; Cherkasov
Russian Chemical Bulletin, 2003 , vol. 52, # 4 p. 910 - 915
