4-甲基-4-戊烯酸乙酯合成路线 （共 22 条）
反应条件
propionic acid 8 h; Reflux;
参考文献
Cai, Zhengxin; Yongpruksa, Nattawut; Harmata, Michael
Organic Letters, 2012 , vol. 14, # 7 p. 1661 - 1663
反应条件
1: T=170°C; P=130 Torr; Heating / reflux; 2: With potassium dihydrogenphosphate T=20°C; 1.5 h;
参考文献
PARHAMI, Farhad; KIM, Woo-Kyun
Patent: WO2008/82520 A2, 2008 ;
Location in patent: Page/Page column 40 ;
反应条件
sodium chloride in water; dimethyl sulfoxide 12 h; Heating;
参考文献
Fernandez-Mateos; Herrero Teijon; Mateos Buron; Rabanedo Clemente; Rubio Gonzalez
Journal of Organic Chemistry, 2007 , vol. 72, # 26 p. 9973 - 9982
反应条件
potassium hexamethylsilazane in toluene
参考文献
Demeke, Damtew; Forsyth, Craig J
Tetrahedron, 2002 , vol. 58, # 32 p. 6531 - 6544
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran T=70°C; Negishi cross-coupling; 18 h;
参考文献
Hansen, Anders L.; Ebran, Jean-Philippe; Gogsig, Thomas M.; Skrydstrup, Troels
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6464 - 6472
反应条件
copper acetylacetonate in diethyl ether T=25°C; 2 h;
参考文献
Gaudemar, M.
Tetrahedron Letters, 1983 , vol. 24, # 27 p. 2749 - 2752
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran T=0°C; 12 h; Inert atmosphere;
参考文献
Poth, Dennis; Peram, Pardha Saradhi; Vences, Miguel; Schulz, Stefan
Journal of Natural Products, 2013 , vol. 76, # 9 p. 1548 - 1558
反应条件
in benzene 0.5 h; Irradiation;
参考文献
Watanabe, Yoshihiko; Yoneda, Tetsuo; Okumura, Tatsuya; Ueno, Yoshio; Toru, Takeshi
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3030 - 3033
反应条件
copper T=160 - 162°C;
参考文献
Roustan,J.L. et al.
Journal of Organometallic Chemistry, 1979 , vol. 168, p. 61 - 86
反应条件
palladium dichloride T=100°C; 24 h;
参考文献
Hosaka,S.; Tsuji,J.
Tetrahedron, 1971 , vol. 27, p. 3821 - 3829
