2-巯基-6-硝基苯并噻唑合成路线 (共 18 条)
参考文献
University of Iowa Research Foundation
Patent: US4975448 A1, 1990 ;
反应条件
in N,N-dimethyl-formamide T=120°C; 0.166667 h; microwave irradiation;
参考文献
Huang, Wei; Tan, Ying; Ding, Ming-Wu; Yang, Guang-Fu
Synthetic Communications, 2007 , vol. 37, # 3 p. 369 - 376
反应条件
sulfuric acid; nitric acid T=0°C; 2 h;
参考文献
Kouge, Katsushige; Koizumi, Tatsuya; Ishibashi, Norio; Okai, Hideo
Agricultural and Biological Chemistry, 1987 , vol. 51, # 7 p. 1941 - 1946
参考文献
Scott; Watt
Journal of Organic Chemistry, 1937 , vol. 2, p. 148,153
反应条件
1: NaOH; aqueous O-butyl-diethylene glycol 2: acetic acid; aqueous KMnO4 View Scheme
参考文献
Cutter; Golden
Journal of the American Chemical Society, 1947 , vol. 69, p. 831
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Korman
Journal of Organic Chemistry, 1958 , vol. 23, p. 1768,1771
反应条件
hydrogenchloride; iron in ethanol; water T=40°C; 0.75 h;
参考文献
Samanta, Sanjay; Lim, Ting Liang; Lam, Yulin
ChemMedChem, 2013 , vol. 8, # 6 p. 994 - 1001
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 8 p. 3229 - 3231
反应条件
in water; N,N-dimethyl-formamide
参考文献
Cutter; Golden
Journal of the American Chemical Society, 1947 , vol. 69, p. 831
参考文献
Takahashi; Numata
Yakugaku Zasshi, 1946 , vol. 66, p. Ausg. B, S. 75
Chem.Abstr., 1952 , p. 112