2-乙基吡啶 1-氧化物合成路线 （共 13 条）
反应条件
1: sulfuric acid; nitric acid 2: iron; concentrated aqueous HCl; acetic acid 3: bromine; aqueous sodium nitrite solution; aqueous hydrobromic acid 4: 160 - 170 °C 5: pyridine; triethylamine / Einleiten von H2S View Scheme
参考文献
Kutscherowa et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 915,918; engl. Ausg. S. 898
反应条件
in 1,2-dichloro-ethane 2 h; Heating; MechanismProduct distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 10 p. 3020 - 3028
反应条件
T=800°C; P=0.1 Torr;
参考文献
Ohsawa, Akio; Kawaguchi, Takayuki; Igeta, Hiroshi
Chemistry Letters, 1981 , p. 1737 - 1738
反应条件
in 1,2-dichloro-ethane 2 h; Heating; MechanismProduct distribution;
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 10 p. 3020 - 3028
反应条件
1: H2SO4; HNO3 2: acetic anhydride View Scheme
参考文献
Karlin, Kenneth D.; Zhang, Christiana Xin; Rheingold, Arnold L.; Galliker, Benedikt; Kaderli, Susan; Zuberbuehler, Andreas D.
Inorganica Chimica Acta, 2012 , vol. 389, p. 138 - 150
反应条件
1: sulfuric acid; nitric acid 2: iron; concentrated aqueous HCl; acetic acid 3: bromine; aqueous sodium nitrite solution; aqueous hydrobromic acid 4: 160 - 170 °C View Scheme
参考文献
Kutscherowa et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 915,918; engl. Ausg. S. 898
反应条件
1: sulfuric acid; nitric acid 2: iron; concentrated aqueous HCl; acetic acid 3: bromine; aqueous sodium nitrite solution; aqueous hydrobromic acid View Scheme
参考文献
Kutscherowa et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 915,918; engl. Ausg. S. 898
反应条件
dihydrogen peroxide; acetic acid
T=80°C;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; WUNBERG, Tobias; SCHNEIDER, Siegfried; VAN DER VEEN, Lars
Patent: WO2010/122069 A1, 2010 ;
Location in patent: Page/Page column 23-24 ;
WO 2010/122069 A1
反应条件
nicotinamide; sodium phosphate buffer; G6P; NADP; magnesium chloride in water
T=37°C; 1 h; biotransformation with phenobarbital-pretreated rat-liver (S-9);
参考文献
Takeshita, Mitsuhiro; Miura, Masatomo; Unuma, Yukiko; Iwai, Sakiko; Sato, Izumi; Hongo, Takahiko; Arai, Toshie; Kosaka, Kazuhiro
Heterocycles, 1996 , vol. 42, # 2 p. 831 - 836
反应条件
1: sulfuric acid; nitric acid
2: iron; concentrated aqueous HCl; acetic acid
3: sodium nitrite; concentrated aqueous hydrochloric acid
View Scheme
参考文献
Kutscherowa et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 915,918; engl. Ausg. S. 898
