2.6-DICYCLOHEXYLPHENOL合成路线 (共 12 条)
反应条件
hydrazine hydrate; palladium on activated charcoal in ethanol
参考文献
Wagner,E.R. et al.
Journal of Medicinal Chemistry, 1977 , vol. 20, p. 1007 - 1013
反应条件
1: H2SO4 2: aq. N2H4 / Pd-C / ethanol View Scheme
参考文献
Wagner,E.R. et al.
Journal of Medicinal Chemistry, 1977 , vol. 20, p. 1007 - 1013
参考文献
Farbenfabr. Bayer
Patent: DE944014 , 1954 ;
反应条件
T=110 - 120°C; 96 h;
参考文献
Arredondo, Yolanda; Moreno-Manas, Marcial; Pleixats, Roser
Synthetic Communications, 1996 , vol. 26, # 21 p. 3885 - 3895
反应条件
1-butyl-3-methylimidazolium heptachlorodiindate (III) T=120°C; 4 h; In ionic liquid; Product distribution / selectivity;
参考文献
SCHENECTADY INTERNATIONAL, INC.
Patent: WO2006/74401 A1, 2006 ;
Location in patent: Page/Page column 18-19 ;
反应条件
deuterium in toluene 900 psi, 80°C for 24 h; (1)H-NMR;
参考文献
Steffey, Bryan D.; Rothwell, Ian P.
Journal of the Chemical Society, Chemical Communications, 1990 , # 3 p. 213 - 215
反应条件
aluminium phenoxide T=200°C; 8 h;
参考文献
Kozlikovskii, Ya. B.; Koshchii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 108 - 111
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 121 - 124
反应条件
(i) Al, (ii) /BRN= 906737/; Multistep reaction;
参考文献
Oleynik; Kuprina; Pevneva; Markov; Kandalintseva; Prosenko; Grigor'ev
Russian Chemical Bulletin, 2007 , vol. 56, # 6 p. 1135 - 1143
反应条件
aluminium phenoxide T=190°C; 2 h; other time, other temperature. Other object of study: mechanism; Thermodynamic dataKineticsRate constant;
参考文献
Kozlikovskii, Ya. B.; Koshchii, V. A.; Chernyaev, B. V.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 909 - 913
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 1014 - 1020
反应条件
T=244°C; unter Druck;
参考文献
Kolka et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 642,645